[RuHCl(CCH₂)(P(C₆H₁₁)3)2]

Base Information

Chemical Name:[RuHCl(CCH₂)(P(C₆H₁₁)3)2]
CAS No.:209330-49-4
Molecular Formula:C₃₈H₆₉ClP₂Ru
Molecular Weight:724.436
Hs Code.:

[RuHCl(CCH<sub>2</sub>)(P(C<sub>6</sub>H<sub>11</sub>)3)2]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [RuHCl(CCH₂)(P(C₆H₁₁)3)2]

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Technology Process of [RuHCl(CCH₂)(P(C₆H₁₁)3)2]

There total 1 articles about [RuHCl(CCH₂)(P(C₆H₁₁)3)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 315675-18-4,133779-04-1
RuHCl(H₂)(PCy₃)2

: 74-86-2,25067-58-7
acetylene

: 209330-49-4
[RuHCl(CCH₂)(P(C₆H₁₁)3)2]

Guidance literature:: In dichloromethane; under Ar; stream of acetylene passed through soln. of Ru complex in CH2Cl2 at -78°C for ca. 10 s; evapd. under vac., residue washed twice with pentane at -20°C, dried under vac.; elem. anal.;
DOI:10.1039/b502440d

Reference yield: 99.0%

: 209330-49-4
[RuHCl(CCH₂)(P(C₆H₁₁)3)2]

: tricyclohexylphosphonium chloride

: [RuCl₂(=CHCH₃)(PCy₃)2]

Guidance literature:: In dichloromethane; Ar atm.; excess of HP(C6H11)3Cl and Ru complex in CH2Cl2;
DOI:10.1039/b502440d

Reference yield: 94.0%

: 209330-49-4
[RuHCl(CCH₂)(P(C₆H₁₁)3)2]

: 7698-05-7
hydrogen chloride

: [RuCl₂(CHCH₂⁽²⁾H)(P(C₆H₁₁)3)2]

Guidance literature:: In water-d2; benzene; Ar atm.; soln. of Ru complex in benzene treated with a 37% DCl in D2O atroom temp., mixt. stirred for 5 min; evapd. under vac., washed with acetone, dried under vac.;
DOI:10.1039/b502440d