P(C₆H₅)4⁽¹⁺⁾*{MoBr₄(SC₅H₃NHSi(CH₃)3)2}^(1-)={P(C₆H₅)4}{MoBr₄(SC₅H₃NHSi(CH₃)3)2}

Base Information

Chemical Name:P(C₆H₅)4⁽¹⁺⁾*{MoBr₄(SC₅H₃NHSi(CH₃)3)2}^(1-)={P(C₆H₅)4}{MoBr₄(SC₅H₃NHSi(CH₃)3)2}
CAS No.:127551-45-5
Molecular Formula:C₁₆H₂₆Br₄MoN₂S₂Si₂*C₂₄H₂₀P
Molecular Weight:1121.65
Hs Code.:

P(C<sub>6</sub>H<sub>5</sub>)4<sup>(1+)</sup>*{MoBr<sub>4</sub>(SC<sub>5</sub>H<sub>3</sub>NHSi(CH<sub>3</sub>)3)2}<sup>(1-)</sup>={P(C<sub>6</sub>H<sub>5</sub>)4}{MoBr<sub>4</sub>(SC<sub>5</sub>H<sub>3</sub>NHSi(CH<sub>3</sub>)3)2}

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Chemical Property of P(C₆H₅)4⁽¹⁺⁾*{MoBr₄(SC₅H₃NHSi(CH₃)3)2}^(1-)={P(C₆H₅)4}{MoBr₄(SC₅H₃NHSi(CH₃)3)2}

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Technology Process of P(C₆H₅)4⁽¹⁺⁾*{MoBr₄(SC₅H₃NHSi(CH₃)3)2}^(1-)={P(C₆H₅)4}{MoBr₄(SC₅H₃NHSi(CH₃)3)2}

There total 1 articles about P(C₆H₅)4⁽¹⁺⁾*{MoBr₄(SC₅H₃NHSi(CH₃)3)2}^(1-)={P(C₆H₅)4}{MoBr₄(SC₅H₃NHSi(CH₃)3)2} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 22172-30-1
dibromotetracarbonylmolybdenum(II)

: 2751-90-8
tetraphenylphosphonium bromide

: 116725-49-6
3-trimethylsilylpyridine-2-thiol

: 127551-45-5
P(C₆H₅)4⁽¹⁺⁾*{MoBr₄(SC₅H₃NHSi(CH₃)3)2}^(1-)={P(C₆H₅)4}{MoBr₄(SC₅H₃NHSi(CH₃)3)2}

: P(C₆H₅)4⁽¹⁺⁾*{MoOBr₃(SC₅H₃NSi(CH₃)3)}^(1-)={P(C₆H₅)4}{MoOBr₃(SC₅H₃NSi(CH₃)3)}

Guidance literature:: In acetonitrile; MoBr2(CO)4 is added to a soln. of HSC5H3N-3-SiMe3 in acetonitrile, a deep red soln. is obtained, addn. of Ph4PBr, stirring for 24 h at room temp.; evapn. to dryness, recrystn. (CH3OH/Et2O) yielding the MoBr4(thiol)2 complex; on treating the filtrate with CH2Cl2 and standing for 2 weeks the MoOBr3-thiolate complex is formed;
DOI:10.1016/S0020-1693(00)80488-0

Reference yield: 20.0%

: 127551-45-5
P(C₆H₅)4⁽¹⁺⁾*{MoBr₄(SC₅H₃NHSi(CH₃)3)2}^(1-)={P(C₆H₅)4}{MoBr₄(SC₅H₃NHSi(CH₃)3)2}

: 618-40-6
1-Methyl-1-phenylhydrazine

: {Mo(SC₅H₃NSi(CH₃)3)2(NN(CH₃)(C₆H₅))2}

Guidance literature:: In dichloromethane; (Ar), a solution of Mo-compound was treated with hydrazine at room temperature while stirred, after 24 h diethyl ether added; evaporated under argon, elem. anal.;