4-Dimethylamino-2-hydroxy-2'-methoxycarbonyl-4'-nitrobenzophenone

Base Information

Chemical Name:4-Dimethylamino-2-hydroxy-2'-methoxycarbonyl-4'-nitrobenzophenone
CAS No.:159435-03-7
Molecular Formula:C₁₇H₁₆N₂O₆
Molecular Weight:344.324
Hs Code.:
DSSTox Substance ID:DTXSID40391868
Wikidata:Q82189622
Mol file:159435-03-7.mol

Synonyms:159435-03-7;4-DIMETHYLAMINO-2-HYDROXY-2'-METHOXYCARBONYL-4'-NITROBENZOPHENONE;methyl 2-[4-(dimethylamino)-2-hydroxybenzoyl]-5-nitrobenzoate;DTXSID40391868;QZWNCXYWULFBHZ-UHFFFAOYSA-N;AKOS030254247;FT-0667276;4-Dimethylamino-2-hydroxy-2'methoxycarbonyl-4'-nitrobenzophenone;4-Dimethylamino-2-hydroxy-2 inverted exclamation mark -methoxycarbonyl-4 inverted exclamation mark -nitrobenzophenone

Suppliers and Price of 4-Dimethylamino-2-hydroxy-2'-methoxycarbonyl-4'-nitrobenzophenone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
4-Dimethylamino-2-hydroxy-2’-methoxycarbonyl-4’-nitrobenzophenone
50mg
$ 120.00

Biosynth Carbosynth
4-Dimethylamino-2-hydroxy-2'-methoxycarbonyl-4'-nitrobenzophenone
25 mg
$ 110.00

Biosynth Carbosynth
4-Dimethylamino-2-hydroxy-2'-methoxycarbonyl-4'-nitrobenzophenone
500 mg
$ 1205.00

Biosynth Carbosynth
4-Dimethylamino-2-hydroxy-2'-methoxycarbonyl-4'-nitrobenzophenone
250 mg
$ 662.50

Biosynth Carbosynth
4-Dimethylamino-2-hydroxy-2'-methoxycarbonyl-4'-nitrobenzophenone
100 mg
$ 364.00

Biosynth Carbosynth
4-Dimethylamino-2-hydroxy-2'-methoxycarbonyl-4'-nitrobenzophenone
50 mg
$ 200.50

Total 6 raw suppliers

Chemical Property of 4-Dimethylamino-2-hydroxy-2'-methoxycarbonyl-4'-nitrobenzophenone

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:5
Exact Mass:344.10083623
Heavy Atom Count:25
Complexity:518

Purity/Quality:

99% ^*data from raw suppliers

4-Dimethylamino-2-hydroxy-2’-methoxycarbonyl-4’-nitrobenzophenone ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C)C1=CC(=C(C=C1)C(=O)C2=C(C=C(C=C2)[N+](=O)[O-])C(=O)OC)O
Uses 4-DIMETHYLAMINO-2-HYDROXY-2'-METHOXYCARBONYL-4'-NITROBENZOPHENONE is Synthetic Intermediat 4-DIMETHYLAMINO-2-HYDROXY-2'-METHOXYCARBONYL-4'-NITROBENZOPHENONE is an intermediate used for the preparation of rhodamine derivatives as fluorescent labels.

Technology Process of 4-Dimethylamino-2-hydroxy-2'-methoxycarbonyl-4'-nitrobenzophenone

There total 2 articles about 4-Dimethylamino-2-hydroxy-2'-methoxycarbonyl-4'-nitrobenzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 3.0%

: 67-56-1
methanol

: 5466-84-2
4-nitrophthalic anhydride

: 99-07-0
3-Dimethylaminophenol

: 159435-02-6
methyl 2-(4'-dimethylamino-2'-hydroxybenzoyl)-4-nitrobenzoate

: 159435-03-7
methyl 2-(4'-dimethylamino-2'-hydroxybenzoyl)-5-nitrobenzoate

Guidance literature:: With sulfuric acid; Yield given. Multistep reaction; 1) toluene, reflux, 6 h; 2) reflux, 8 h;

Reference yield:

: 610-27-5
4-nitrophthalic acid

: 159435-03-7
methyl 2-(4'-dimethylamino-2'-hydroxybenzoyl)-5-nitrobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / acetic anhydride / 1) 60 deg C, 1 h; 2) reflux, 10 min

2: 2.) conc. H₂SO₄ / 1) toluene, reflux, 6 h; 2) reflux, 8 h

With sulfuric acid; acetic anhydride;