N¹-benzyl-N²-(5-methyl-[1,1'-biphenyl]-2-yl)oxalamide

Base Information

• Chemical Name: N¹-benzyl-N²-(5-methyl-[1,1'-biphenyl]-2-yl)oxalamide
• CAS No.: 1909333-82-9
• Molecular Formula: C₂₂H₂₀N₂O₂
• Molecular Weight: 344.413

Synonyms:

Chemical Property of N¹-benzyl-N²-(5-methyl-[1,1'-biphenyl]-2-yl)oxalamide

Chemical Property:

• Density: 1.199±0.06 g/cm3(Predicted)

Purity/Quality:

99%, ^*data from raw suppliers

N1-benzyl-n2-(5-methyl-2-biphenylyl)oxalamide 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N¹-benzyl-N²-(5-methyl-[1,1'-biphenyl]-2-yl)oxalamide

There total 6 articles about N¹-benzyl-N²-(5-methyl-[1,1'-biphenyl]-2-yl)oxalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

C16H15NO3 + benzylamine (100-46-9) → N1-benzyl-N2-(5-methyl-[1,1'-biphenyl]-2-yl)oxalamide (1909333-82-9)

Guidance literature:

In tetrahydrofuran; at 70 ℃; for 2h;

DOI:10.1021/acs.orglett.7b02326

Reference yield: 85.0%

monomethyl oxalyl chloride (5781-53-3) + 2-amino-5-methylbiphenyl (42308-28-1) + benzylamine (100-46-9) → N1-benzyl-N2-(5-methyl-[1,1'-biphenyl]-2-yl)oxalamide (1909333-82-9)

Guidance literature:

monomethyl oxalyl chloride; 2-amino-5-methylbiphenyl; With triethylamine; In tetrahydrofuran; at 20 ℃; Cooling with ice;

benzylamine; In tetrahydrofuran; at 20 - 70 ℃; for 2h;

DOI:10.1021/jacs.8b12142

Reference yield:

oxalyl dichloride (79-37-8) + 2-amino-5-methylbiphenyl (42308-28-1) + benzylamine (100-46-9) → N1-benzyl-N2-(5-methyl-[1,1'-biphenyl]-2-yl)oxalamide (1909333-82-9)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 2h;

DOI:10.1002/adsc.201700026

upstream raw materials:

benzylamine

2-amino-5-methylbiphenyl

oxalyl dichloride

phenylboronic acid

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