Technology Process of C37H32O9S2
There total 5 articles about C37H32O9S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine / 4 h / Ambient temperature
2: 91 percent / H2 / 10percent Pd/C / methanol; dimethylformamide / 25 h
3: 1.) NaH / 1.) DMF, 0 deg C, 30 min, 2.) DMF, 0 deg C, 30 min
With
pyridine; hydrogen; sodium hydride;
palladium on activated charcoal;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1135/cccc19982044
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 9 percent / LiAlH4 / tetrahydrofuran / 2 h / Heating
2: pyridine / 4 h / Ambient temperature
3: 91 percent / H2 / 10percent Pd/C / methanol; dimethylformamide / 25 h
4: 1.) NaH / 1.) DMF, 0 deg C, 30 min, 2.) DMF, 0 deg C, 30 min
With
pyridine; lithium aluminium tetrahydride; hydrogen; sodium hydride;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1135/cccc19982044
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine / 4 h / Ambient temperature
2: 91 percent / H2 / 10percent Pd/C / methanol; dimethylformamide / 25 h
3: 1.) NaH / 1.) DMF, 0 deg C, 30 min, 2.) DMF, 0 deg C, 30 min
With
pyridine; hydrogen; sodium hydride;
palladium on activated charcoal;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1135/cccc19982044