fac-Mo(CO)3(bipy)P(p-C₆H₄Cl)3

Base Information

Chemical Name:fac-Mo(CO)3(bipy)P(p-C₆H₄Cl)3
CAS No.:91357-69-6
Molecular Formula:C₃₁H₂₀Cl₃MoN₂O₃P
Molecular Weight:701.784
Hs Code.:

fac-Mo(CO)3(bipy)P(p-C<sub>6</sub>H<sub>4</sub>Cl)3

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Chemical Property of fac-Mo(CO)3(bipy)P(p-C₆H₄Cl)3

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Technology Process of fac-Mo(CO)3(bipy)P(p-C₆H₄Cl)3

There total 1 articles about fac-Mo(CO)3(bipy)P(p-C₆H₄Cl)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15668-64-1
tetracarbonyl(2,2'-bipyridine)molybdenum

: 1159-54-2
tri(4-chlorophenyl)phosphine

: 91357-69-6
fac-Mo(CO)3(bipy)P(p-C₆H₄Cl)3

Guidance literature:: In not given; byproducts: CO; according to the method by M. H. B. Stiddard, J. Chem. Soc. (1963) 756; elem. anal.;
DOI:10.1016/0022-328X(84)80137-0

Reference yield:

: 91357-69-6
(C₅H₄NC₅H₄N)(P(C₆H₄Cl)3)Mo(CO)3

: 993-16-8
methyltin(IV) trichloride

: (C₅H₄NC₅H₄N)(P(C₆H₄Cl)3)(CO)2Mo(Cl)(SnCl₂CH₃)

Guidance literature:: In acetone; a soln. of MeSnCl3 in acetone was added to Mo-complex under N2, the stirred mixt. was refluxed under N2 for 12 h; soln. was cooled to room temp., ppt. was filtered off, washed with warmacetone/ethanol, dried in vacuo; elem. anal.;
DOI:10.1016/0022-328X(85)87258-2

Reference yield:

: 91357-69-6
(C₅H₄NC₅H₄N)(P(C₆H₄Cl)3)Mo(CO)3

: 7646-78-8
tin(IV) chloride

: (C₅H₄NC₅H₄N)(P(C₆H₄Cl)3)(CO)2Mo(Cl)(SnCl₃)

Guidance literature:: In dichloromethane; acetone; byproducts: CO; a soln. of SnCl4 in acetone-CH2Cl2 was added to Mo-complex under N2, mixt. was stirred at room temp. for 70 h; ppt. was filtered, washed with acetone and ether, dried in vacuo; elem.anal.;
DOI:10.1016/0022-328X(85)87258-2