C₁₈H₃₇NO₁₃P₂

Base Information

• Chemical Name: C₁₈H₃₇NO₁₃P₂
• CAS No.: 1412439-51-0
• Molecular Formula: C₁₈H₃₇NO₁₃P₂
• Molecular Weight: 537.438
• Mol file: 1412439-51-0.mol

Synonyms:

Chemical Property of C₁₈H₃₇NO₁₃P₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₈H₃₇NO₁₃P₂

There total 17 articles about C₁₈H₃₇NO₁₃P₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1D-1-O-(tert-butyldiphenylsilyl)-2,3,6-O-tris(methoxymethylene)-myo-inositol 4,5-bis(dibenzylphosphate) (496808-68-5) → C18H37NO13P2 (1412439-51-0)

Guidance literature:

Multi-step reaction with 4 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 72 h / 20 °C / Inert atmosphere

3: trimethylsilyl bromide / dichloromethane / 2 h / -78 °C / Inert atmosphere; Darkness

4: methanol / 1 h / 20 °C

With methanol; dmap; trimethylsilyl bromide; tetrabutyl ammonium fluoride; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane;

DOI:10.1002/ejoc.201200726

Reference yield:

methyl 12-(benzyloxycarbonylamino)dodecanoate (1129295-44-8) → C18H37NO13P2 (1412439-51-0)

Guidance literature:

Multi-step reaction with 4 steps

1: lithium hydroxide / water; tetrahydrofuran / 10 h / 20 °C

2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 72 h / 20 °C / Inert atmosphere

3: trimethylsilyl bromide / dichloromethane / 2 h / -78 °C / Inert atmosphere; Darkness

4: methanol / 1 h / 20 °C

With methanol; dmap; trimethylsilyl bromide; dicyclohexyl-carbodiimide; lithium hydroxide; In tetrahydrofuran; dichloromethane; water;

DOI:10.1002/ejoc.201200726

Reference yield:

1D-2,3,6-O-tris(methoxymethylene)-myo-inositol 4,5-bis(dibenzyl phosphate) (496808-69-6) → C18H37NO13P2 (1412439-51-0)

Guidance literature:

Multi-step reaction with 3 steps

1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 72 h / 20 °C / Inert atmosphere

2: trimethylsilyl bromide / dichloromethane / 2 h / -78 °C / Inert atmosphere; Darkness

3: methanol / 1 h / 20 °C

With methanol; dmap; trimethylsilyl bromide; dicyclohexyl-carbodiimide; In dichloromethane;

DOI:10.1002/ejoc.201200726

upstream raw materials:

1D-1-O-(tert-butyldiphenylsilyl)-2,3,6-O-tris(methoxymethylene)-myo-inositol 4,5-bis(dibenzylphosphate)

1D-2,3,6-O-tris(methoxymethylene)-myo-inositol 4,5-bis(dibenzyl phosphate)

methyl 12-(benzyloxycarbonylamino)dodecanoate

12-(((benzyloxy)carbonyl)amino)dodecanoic acid