Methyl-3,6-dideoxy-α-D-ribo-hexopivanosid

Base Information

Chemical Name:Methyl-3,6-dideoxy-α-D-ribo-hexopivanosid
CAS No.:64880-44-0
Molecular Formula:C₇H₁₄O₄
Molecular Weight:162.186
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl-3,6-dideoxy-α-D-ribo-hexopivanosid

Chemical Property:

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Technology Process of Methyl-3,6-dideoxy-α-D-ribo-hexopivanosid

There total 2 articles about Methyl-3,6-dideoxy-α-D-ribo-hexopivanosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28251-53-8
methyl 2,3,4-tri-O-acetyl-α-L-rhamnopyranoside

: 18465-83-3
methyl-4,6-dideoxy-α-L-lyxo-hexapyranoside

: 19131-10-3
methyl-2,6-didesoxy-α-L-arabino-hexopyranoside

: 64880-44-0
methyl 3,6-dideoxy-α-L-arabino-hexopyranoside

Guidance literature:: With sodium methylate; Yield given. Multistep reaction. Yields of byproduct given; 1) HMPA, H₂O, irradiation, 12 h, 2) MeOH, 60 deg C, 5 min;
DOI:10.1007/BF00597843

Reference yield:

: 6109-60-0,6109-61-1,6109-62-2,6154-71-8,31505-15-4,31899-66-8,33302-96-4,53294-48-7,64880-44-0,69283-22-3
Methyl-3,6-dideoxy-α-D-ribo-hexopivanosid

Guidance literature:: aus Methyl-2,3,4,6-tetra-O-p-toluensulphonyl-α-D-glucosid (I);

Reference yield:

: 64880-44-0
methyl 3,6-dideoxy-α-L-arabino-hexopyranoside

: 74652-66-7
methyl-5-azido-2-O-benzoyl-3,5,6-tridesoxy-β-D-xylo-hexofuranoside

Guidance literature:: Multi-step reaction with 4 steps

1: aluminium chloride / dioxane

2: 88 percent / hydrogen / 10 percent palladium on carbon / methanol

3: 95 percent / pyridine / Ambient temperature

4: 81 percent / sodium azide / hexamethylphosphoric acid triamide / 2 h / 90 °C

With sodium azide; hydrogen; palladium on activated charcoal; aluminium trichloride; In 1,4-dioxane; pyridine; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide;
DOI:10.1016/S0008-6215(00)85654-2