Technology Process of C32H32O4S2
There total 4 articles about C32H32O4S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C20H14O4S2;
With
potassium carbonate; potassium iodide;
In
N,N-dimethyl-formamide;
at 80 ℃;
for 0.5h;
Inert atmosphere;
1-bromo-4-butene;
In
N,N-dimethyl-formamide;
at 80 ℃;
for 72h;
Inert atmosphere;
DOI:10.1002/asia.201100524
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium(0); potassium phosphate / toluene
2.1: boron tribromide / dichloromethane
3.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 0.5 h / 80 °C / Inert atmosphere
3.2: 72 h / 80 °C / Inert atmosphere
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); boron tribromide; potassium carbonate; potassium iodide;
In
dichloromethane; N,N-dimethyl-formamide; toluene;
1.1: Suzuki-Miyauri coupling / 3.1: Williamson synthesis / 3.2: Williamson synthesis;
DOI:10.1002/asia.201100524
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: boron tribromide / dichloromethane
2.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 0.5 h / 80 °C / Inert atmosphere
2.2: 72 h / 80 °C / Inert atmosphere
With
boron tribromide; potassium carbonate; potassium iodide;
In
dichloromethane; N,N-dimethyl-formamide;
2.1: Williamson synthesis / 2.2: Williamson synthesis;
DOI:10.1002/asia.201100524
