1-Chloro-2,3-dimethylcyclopropane

Base Information

• Chemical Name: 1-Chloro-2,3-dimethylcyclopropane
• CAS No.: 53177-35-8
• Molecular Formula: C₅H₉Cl
• Molecular Weight: 104.579
• NSC Number: 179439
• DSSTox Substance ID: DTXSID50306726

Synonyms:25271-13-0;1-chloro-2,3-dimethylcyclopropane;NSC179439;SCHEMBL16116900;DTXSID50306726;1,2-dimethyl-3-chlorocyclopropane;NSC-179439

Chemical Property of 1-Chloro-2,3-dimethylcyclopropane

Chemical Property:

• XLogP3: 2.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 104.0392780
• Heavy Atom Count: 6
• Complexity: 53

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC1C(C1Cl)C

Technology Process of 1-Chloro-2,3-dimethylcyclopropane

There total 4 articles about 1-Chloro-2,3-dimethylcyclopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trans-2-Butene (624-64-6) + dichloromethane (75-09-2) → 1-Chlor-cis,trans-2,3-dimethylcyclopropan (25271-11-8,25271-12-9,25271-13-0,53177-35-8)

Guidance literature:

With n-butyllithium; at -35 ℃;

DOI:10.1021/ja01527a057 DOI:10.1021/ja01506a041

Reference yield:

→ trans-2.3-Dimethyl-cyclopropylchlorid (25271-11-8,25271-12-9,25271-13-0,53177-35-8)

Guidance literature:

Aus trans-Buten-(2) mit Chlordiazomethan in Ae; -20grad, Pyrolyse;

DOI:10.1021/ja00881a034

Reference yield:

→ 1-Chlor-2,3-trans-dimethylcyclopropan (25271-11-8,25271-12-9,25271-13-0,53177-35-8)

Guidance literature:

Aus trans-Buten-(2), CH2Cl2 u. Butyl-Li; 1-1.5 h, -35grad unter N2;

DOI:10.1021/ja01506a041

upstream raw materials:

trans-2-Butene

dichloromethane

Downstream raw materials:

1-methyl-2-methylenecyclopropane

3-methylcyclobutan-1-one

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