trans 1,2-diphenoxycyclobutane

Base Information

• Chemical Name: trans 1,2-diphenoxycyclobutane
• CAS No.: 35370-70-8
• Molecular Formula: C₁₆H₁₆O₂
• Molecular Weight: 240.302
• Mol file: 35370-70-8.mol

Synonyms:

Chemical Property of trans 1,2-diphenoxycyclobutane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of trans 1,2-diphenoxycyclobutane

There total 3 articles about trans 1,2-diphenoxycyclobutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

vinyl phenyl ether (766-94-9) → cis 1,2-diphenoxycyclobutane (35370-71-9) + trans 1,2-diphenoxycyclobutane (35370-70-8)

Guidance literature:

zinc(II) oxide; In dichloromethane; for 1.5h; Product distribution; Irradiation; further solvents and semiconductors; effect of semiconductor purity and concentration, oxygen and cutoff wavelength; quenching effect of isoprene, methoxybenzenes, methyl alcohol, ethyl vinyl ether, furan and methylfuran;

DOI:10.1021/ja00333a018

Reference yield:

vinyl phenyl ether (766-94-9) → cis 1,2-diphenoxycyclobutane (35370-71-9) + 2-methyl-3-phenoxypyridine (76167-46-9) + trans 1,2-diphenoxycyclobutane (35370-70-8) + phenol (108-95-2,27073-41-2)

Guidance literature:

With poly<2,6-diphenyl-4-(4'-vinylphenyl)pyrylium tetrafluoroborate>; In acetonitrile; for 6h; Product distribution; Irradiation; dimerization with different sensitizers, other times, solvents, conc. of the educt;

Reference yield:

→ vinyl phenyl ether (766-94-9) + trans 1,2-diphenoxycyclobutane (35370-70-8)

Guidance literature:

With 9,10-Dicyanoanthracene; In acetonitrile; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Irradiation;

DOI:10.1021/j150642a003

upstream raw materials:

vinyl phenyl ether