(2S)-N-{4-[6-[2-methoxy-4-((E)-3-oxo-3-[4-(3,4,5-trimethoxybenzoyl)piperazino]-1-propenyl)phenoxy]hexyloxy]-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyl dithioacetal

Base Information

• Chemical Name: (2S)-N-{4-[6-[2-methoxy-4-((E)-3-oxo-3-[4-(3,4,5-trimethoxybenzoyl)piperazino]-1-propenyl)phenoxy]hexyloxy]-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyl dithioacetal
• CAS No.: 1246890-26-5
• Molecular Formula: C₄₇H₆₂N₄O₁₂S₂
• Molecular Weight: 939.161

Synonyms:

Chemical Property of (2S)-N-{4-[6-[2-methoxy-4-((E)-3-oxo-3-[4-(3,4,5-trimethoxybenzoyl)piperazino]-1-propenyl)phenoxy]hexyloxy]-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyl dithioacetal

Chemical Property:

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Useful:

Technology Process of (2S)-N-{4-[6-[2-methoxy-4-((E)-3-oxo-3-[4-(3,4,5-trimethoxybenzoyl)piperazino]-1-propenyl)phenoxy]hexyloxy]-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyl dithioacetal

There total 1 articles about (2S)-N-{4-[6-[2-methoxy-4-((E)-3-oxo-3-[4-(3,4,5-trimethoxybenzoyl)piperazino]-1-propenyl)phenoxy]hexyloxy]-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyl dithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

4-[(6-bromohexyl)oxy]-5-methoxy-2-nitrophenyl2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolylmethanone (1080662-00-5) + (E)-3-(4-hydroxy-3-methoxyphenyl)-1-[4-(3,4,5-trimethoxybenzoyl)piperazino]-2-propen-1-one (1226909-06-3) → (2S)-N-{4-[6-[2-methoxy-4-((E)-3-oxo-3-[4-(3,4,5-trimethoxybenzoyl)piperazino]-1-propenyl)phenoxy]hexyloxy]-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyl dithioacetal (1246890-26-5)

Guidance literature:

With potassium carbonate; In acetonitrile; for 12h; Reflux;

DOI:10.1016/j.ejmech.2010.05.041

Reference yield:

(2S)-N-{4-[6-[2-methoxy-4-((E)-3-oxo-3-[4-(3,4,5-trimethoxybenzoyl)piperazino]-1-propenyl)phenoxy]hexyloxy]-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyl dithioacetal (1246890-26-5) → C47H64N4O10S2

Guidance literature:

With tin(II) chloride hydrate; In methanol; Reflux;

DOI:10.1016/j.ejmech.2010.05.041

upstream raw materials:

4-[(6-bromohexyl)oxy]-5-methoxy-2-nitrophenyl2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolylmethanone

(E)-3-(4-hydroxy-3-methoxyphenyl)-1-[4-(3,4,5-trimethoxybenzoyl)piperazino]-2-propen-1-one

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