1,4-diacetyl-2,3,5,6-tetrachloro-benzene

Base Information

• Chemical Name: 1,4-diacetyl-2,3,5,6-tetrachloro-benzene
• CAS No.: 408523-62-6
• Molecular Formula: C₁₀H₆Cl₄O₂
• Molecular Weight: 299.968
• Mol file: 408523-62-6.mol

Synonyms:

Chemical Property of 1,4-diacetyl-2,3,5,6-tetrachloro-benzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,4-diacetyl-2,3,5,6-tetrachloro-benzene

There total 4 articles about 1,4-diacetyl-2,3,5,6-tetrachloro-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,4-diethylbenzene (105-05-5) → 1,4-diacetyl-2,3,5,6-tetrachloro-benzene (408523-62-6)

Guidance literature:

Multi-step reaction with 3 steps

1: iron; chlorine

2: tetrachloromethane; bromine / Irradiation_.Gluehlampenlicht

3: acetic acid / Erwaermen des Reaktionsprodukts mit wss. HCl und Dioxan und Erwaermen des danach erhaltenen Reaktionsprodukts mit CrO₃ und Essigsaeure

With tetrachloromethane; bromine; chlorine; iron; acetic acid;

DOI:10.1021/ja01159a017

Reference yield:

4-ethylacetophenone (937-30-4) → 1,4-diacetyl-2,3,5,6-tetrachloro-benzene (408523-62-6)

Guidance literature:

Multi-step reaction with 4 steps

1: copper oxide-chromium oxide / unter Druck

2: iron; chlorine

3: tetrachloromethane; bromine / Irradiation_.Gluehlampenlicht

4: acetic acid / Erwaermen des Reaktionsprodukts mit wss. HCl und Dioxan und Erwaermen des danach erhaltenen Reaktionsprodukts mit CrO₃ und Essigsaeure

With tetrachloromethane; copper oxide-chromium oxide; bromine; chlorine; iron; acetic acid;

DOI:10.1021/ja01159a017

Reference yield:

1,4-diethyl-2,3,5,6-tetrachloro-benzene (875839-98-8) → 1,4-diacetyl-2,3,5,6-tetrachloro-benzene (408523-62-6)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrachloromethane; bromine / Irradiation_.Gluehlampenlicht

2: acetic acid / Erwaermen des Reaktionsprodukts mit wss. HCl und Dioxan und Erwaermen des danach erhaltenen Reaktionsprodukts mit CrO₃ und Essigsaeure

With tetrachloromethane; bromine; acetic acid;

DOI:10.1021/ja01159a017

upstream raw materials:

1,4-bis-(1-bromo-ethyl)-2,3,5,6-tetrachloro-benzene

potassium acetate

1,4-diethylbenzene

4-ethylacetophenone