Technology Process of methyl 3-O-benzyl-2,5-di-O-mesyl-α-D-xylofuranoside
There total 10 articles about methyl 3-O-benzyl-2,5-di-O-mesyl-α-D-xylofuranoside which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: NaH / dimethylformamide; tetrahydrofuran
2: 1.) aq. HCl, 2.) NaIO4, 3.) NaBH4 / 1) THF, 2) H2O, MeOH, 3.) MeOH
3: aq. HCl
4: pyridine
With
pyridine; hydrogenchloride; sodium tetrahydroborate; sodium periodate; sodium hydride;
In
tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jo9519423
- Guidance literature:
-
Multi-step reaction with 6 steps
1: CuSO4; sulfuric acid / 12 h / 20 °C
2: 36.1 g / hydrochloric acid / H2O / 1.5 h / 20 °C
3: 98 percent / imidazole / dimethylformamide / 1 h / 0 °C
4: 98 percent / sodium hydride / dimethylformamide / 1 h / 0 °C
5: hydrogen chloride / methanol / 3 h / 20 °C
6: pyridine / 0 - 20 °C
With
pyridine; 1H-imidazole; hydrogenchloride; sulfuric acid; sodium hydride; copper(II) sulfate;
In
methanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2005.08.040
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 98 percent / imidazole / dimethylformamide / 1 h / 0 °C
2: 98 percent / sodium hydride / dimethylformamide / 1 h / 0 °C
3: hydrogen chloride / methanol / 3 h / 20 °C
4: pyridine / 0 - 20 °C
With
pyridine; 1H-imidazole; hydrogenchloride; sodium hydride;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2005.08.040
