isobutyl trimethylsilyl S-phenyl phosphorothioate

Base Information

• Chemical Name: isobutyl trimethylsilyl S-phenyl phosphorothioate
• CAS No.: 87515-39-7
• Molecular Formula: C₁₃H₂₃O₃PSSi
• Molecular Weight: 318.449
• Mol file: 87515-39-7.mol

Synonyms:

Chemical Property of isobutyl trimethylsilyl S-phenyl phosphorothioate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of isobutyl trimethylsilyl S-phenyl phosphorothioate

There total 2 articles about isobutyl trimethylsilyl S-phenyl phosphorothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

thiophenol (108-98-5) → isobutyl trimethylsilyl S-phenyl phosphorothioate (87515-39-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 93 percent / triethylamine / benzene / 2 h / Ambient temperature

2: 1.) 0.5 M LiOH, 0.1 M HCl; 2.) triethylamine / 1.) pyridine, RT, 10 min; 2.) benzene, RT, 1 h

With hydrogenchloride; lithium hydroxide; triethylamine; In benzene;

DOI:10.1246/cl.1983.951

Reference yield:

chloro-trimethyl-silane (75-77-4) + isobutyl S,S-diphenyl phosphorodithioate (87515-38-6) → isobutyl trimethylsilyl S-phenyl phosphorothioate (87515-39-7)

Guidance literature:

With hydrogenchloride; lithium hydroxide; triethylamine; Yield given. Multistep reaction; 1.) pyridine, RT, 10 min; 2.) benzene, RT, 1 h;

DOI:10.1246/cl.1983.951

upstream raw materials:

chloro-trimethyl-silane

isobutyl S,S-diphenyl phosphorodithioate

thiophenol