Technology Process of C9H6ClNO
There total 5 articles about C9H6ClNO which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
bis(triphenylphosphine)palladium(II) dichloride; triethylamine;
In
N,N-dimethyl-formamide;
at 20 - 140 ℃;
for 3h;
optical yield given as %de;
Inert atmosphere;
DOI:10.1021/ja2058583
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogenchloride; sodium nitrite / water / 1 h / 0 °C
1.2: 1 h / 60 - 80 °C
2.1: boron tribromide / dichloromethane / 13 h / -78 - 20 °C / Inert atmosphere
3.1: bis(triphenylphosphine)palladium(II) dichloride; triethylamine / N,N-dimethyl-formamide / 3 h / 20 - 140 °C / Inert atmosphere
With
hydrogenchloride; bis(triphenylphosphine)palladium(II) dichloride; boron tribromide; triethylamine; sodium nitrite;
In
dichloromethane; water; N,N-dimethyl-formamide;
3.1: Heck reaction;
DOI:10.1021/ja2058583
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: methanol / 24 h / Reflux
2.1: iron; ammonium chloride / ethanol; water / 4 h / 75 °C
3.1: hydrogenchloride; sodium nitrite / water / 1 h / 0 °C
3.2: 1 h / 60 - 80 °C
4.1: boron tribromide / dichloromethane / 13 h / -78 - 20 °C / Inert atmosphere
5.1: bis(triphenylphosphine)palladium(II) dichloride; triethylamine / N,N-dimethyl-formamide / 3 h / 20 - 140 °C / Inert atmosphere
With
hydrogenchloride; bis(triphenylphosphine)palladium(II) dichloride; boron tribromide; iron; ammonium chloride; triethylamine; sodium nitrite;
In
methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
5.1: Heck reaction;
DOI:10.1021/ja2058583
