(3R)-α--3-bromo-N-(diphenylmethyl)-2-oxo-1-azetidineacetamide

Base Information

Chemical Name:(3R)-α--3-bromo-N-(diphenylmethyl)-2-oxo-1-azetidineacetamide
CAS No.:88147-47-1
Molecular Formula:C₃₁H₂₇BrN₂O₃
Molecular Weight:555.471
Hs Code.:

(3R)-α-<p-(benzyloxy)phenyl>-3-bromo-N-(diphenylmethyl)-2-oxo-1-azetidineacetamide

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Chemical Property of (3R)-α--3-bromo-N-(diphenylmethyl)-2-oxo-1-azetidineacetamide

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Technology Process of (3R)-α--3-bromo-N-(diphenylmethyl)-2-oxo-1-azetidineacetamide

There total 3 articles about (3R)-α--3-bromo-N-(diphenylmethyl)-2-oxo-1-azetidineacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 88147-46-0,88147-51-7,88147-52-8,88156-50-7
(3S)-α-<(p-benzyloxy)phenyl>-N-(diphenylmethyl)-3-hydroxy-2-oxo-1-azedineacetamide

: 88147-47-1,88147-48-2
(3R)-α--3-bromo-N-(diphenylmethyl)-2-oxo-1-azetidineacetamide

Guidance literature:: With methyl bromide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; benzene; for 2.5h; Ambient temperature;
DOI:10.1016/S0040-4020(01)92152-0

Reference yield:

: 4397-53-9
p-benzyloxybenzaldehyde

: 88147-47-1,88147-48-2
(3R)-α--3-bromo-N-(diphenylmethyl)-2-oxo-1-azetidineacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: MeOH/H₂O, reflux, 3 d

2: 57 percent / triphenylphosphine, diethyl azodicarboxylate, MeBr / benzene; tetrahydrofuran / 2.5 h / Ambient temperature

With methyl bromide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; benzene;
DOI:10.1016/S0040-4020(01)92152-0

Reference yield:

: 3128-85-6
diphenylmethyl isocyanide

: 88147-47-1,88147-48-2
(3R)-α--3-bromo-N-(diphenylmethyl)-2-oxo-1-azetidineacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: MeOH/H₂O, reflux, 3 d

2: 57 percent / triphenylphosphine, diethyl azodicarboxylate, MeBr / benzene; tetrahydrofuran / 2.5 h / Ambient temperature

With methyl bromide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; benzene;
DOI:10.1016/S0040-4020(01)92152-0