trans-dichlorobis(2,2'-bipyridyl)ruthenium(II)

Base Information

Chemical Name:trans-dichlorobis(2,2'-bipyridyl)ruthenium(II)
CAS No.:158060-65-2
Molecular Formula:C₂₀H₁₆Cl₂N₄Ru
Molecular Weight:484.35
Hs Code.:

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Chemical Property of trans-dichlorobis(2,2'-bipyridyl)ruthenium(II)

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Technology Process of trans-dichlorobis(2,2'-bipyridyl)ruthenium(II)

There total 46 articles about trans-dichlorobis(2,2'-bipyridyl)ruthenium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 366-18-7
[2,2]bipyridinyl

: dichloro(1,5-cyclooctadiene)ruthenium(II)

: 345911-20-8,19542-80-4,158060-65-2,34795-02-3,15746-57-3
cis-dichlorobis(2,2′-bipyridine)ruthenium(II)

Guidance literature:: In N,N-dimethyl-formamide; other Radiation; a suspn. of Ru-complex and bipyridine-compound in DMF was reacted for 45min under microwave irradiation (microwave set-up; 30 s, 600 W; 45 min, 200 W; 10 min, ventilation); the solvent was immediately removed on the rotary evaporator, the solid was washed with diethyl ether and dried on air;
DOI:10.1016/j.ica.2004.07.007

Reference yield: 90.0%

: Ru((C₅H₄N)2)2Cl₂⁽¹⁺⁾*Cl^(1-)*2H₂O = {Ru((C₅H₄N)2)2Cl₂}Cl*2H₂O

: 345911-20-8,19542-80-4,158060-65-2,34795-02-3,15746-57-3
cis-dichlorobis(2,2′-bipyridine)ruthenium(II)

Guidance literature:: With SnCl₂*2HCl; In hydrogenchloride; SnCl2*2HCl added to a soln. of Ru-compd. in HCl; concd. by warming, washed with H2O, air dried;
DOI:10.1016/S0020-1693(00)85316-5