(1'R*,2'R*)-(E)-1-(2'-t-butyldimethylsiloxymethyl-1',2'-dimethylcyclopentyl)-6-<2,5-bis(methoxymethoxy)-3-methylphenyl>-4-methyl-4-hexen-2-yl pivalate

Base Information

• Chemical Name: (1'R*,2'R*)-(E)-1-(2'-t-butyldimethylsiloxymethyl-1',2'-dimethylcyclopentyl)-6-<2,5-bis(methoxymethoxy)-3-methylphenyl>-4-methyl-4-hexen-2-yl pivalate
• CAS No.: 125318-37-8
• Molecular Formula: C₃₇H₆₄O₇Si
• Molecular Weight: 648.996

Synonyms:

Chemical Property of (1'R*,2'R*)-(E)-1-(2'-t-butyldimethylsiloxymethyl-1',2'-dimethylcyclopentyl)-6-<2,5-bis(methoxymethoxy)-3-methylphenyl>-4-methyl-4-hexen-2-yl pivalate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (1'R*,2'R*)-(E)-1-(2'-t-butyldimethylsiloxymethyl-1',2'-dimethylcyclopentyl)-6-<2,5-bis(methoxymethoxy)-3-methylphenyl>-4-methyl-4-hexen-2-yl pivalate

There total 59 articles about (1'R*,2'R*)-(E)-1-(2'-t-butyldimethylsiloxymethyl-1',2'-dimethylcyclopentyl)-6-<2,5-bis(methoxymethoxy)-3-methylphenyl>-4-methyl-4-hexen-2-yl pivalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

pivaloyl chloride (3282-30-2) + (1'R*,2'R*)-(Z)-1-(2'-t-butyldimethylsiloxymethyl-1',2'-dimethylcyclopentyl)-6-<2,5-bis(methoxymethoxy)-3-methylphenyl>-4-methyl-4-hexen-2-ol (125318-36-7,125410-04-0,125410-14-2,125410-16-4,130852-42-5,130852-55-0) → (1'R*,2'R*)-(Z)-1-(2'-t-butyldimethylsiloxymethyl-1',2'-dimethylcyclopentyl)-6-<2,5-bis(methoxymethoxy)-3-methylphenyl>-4-methyl-4-hexen-2-yl pivalate (125318-37-8,125410-05-1,125410-09-5,125410-12-0,130852-43-6,130852-56-1)

Guidance literature:

With pyridine; dmap; Ambient temperature;

DOI:10.1016/S0040-4020(01)80058-2

Reference yield: 96.0%

(1'R,2'R,4E)-1-(2'-t-butyldimethylsiloxymethyl-1',2'-dimethylcyclopentyl)-6-<2,5-bis(methoxymethoxy)-3-methylphenyl>-4-methyl-4-hexen-2-ol (125318-36-7,125410-04-0,125410-14-2,125410-16-4,130852-42-5,130852-55-0) + pivaloyl chloride (3282-30-2) → (1'R,2'R,4E)-1-(2'-t-butyldimethylsiloxymethyl-1',2'-dimethylcyclopentyl)-6-<2,5-bis(methoxymethoxy)-3-methylphenyl>-4-methyl-4-hexen-2-yl pivalate (125318-37-8,125410-05-1,125410-09-5,125410-12-0,130852-43-6,130852-56-1)

Guidance literature:

With pyridine; dmap; Ambient temperature;

DOI:10.1016/S0040-4020(01)86756-9

Reference yield: 94.0%

pivaloyl chloride (3282-30-2) + (1'R*,2'R*)-(E)-1-(2'-t-butyldimethylsiloxymethyl-1',2'-dimethylcyclopentyl)-6-<2,5-bis(methoxymethoxy)-3-methylphenyl>-4-methyl-4-hexen-2-ol (125318-36-7,125410-04-0,125410-14-2,125410-16-4,130852-42-5,130852-55-0) → (1'R*,2'R*)-(E)-1-(2'-t-butyldimethylsiloxymethyl-1',2'-dimethylcyclopentyl)-6-<2,5-bis(methoxymethoxy)-3-methylphenyl>-4-methyl-4-hexen-2-yl pivalate (125318-37-8,125410-05-1,125410-09-5,125410-12-0,130852-43-6,130852-56-1)

Guidance literature:

With pyridine; dmap; Ambient temperature;

DOI:10.1016/S0040-4020(01)80058-2

upstream raw materials:

(1'R,2'R,4E)-1-(2'-t-butyldimethylsiloxymethyl-1',2'-dimethylcyclopentyl)-6-<2,5-bis(methoxymethoxy)-3-methylphenyl>-4-methyl-4-hexen-2-ol

pivaloyl chloride

(1R*,6R*)-1,6-dimethyl-3-oxabicyclo<4.3.0>nonan-4-one

(1R,2R)-2-t-butyldimethylsiloxymethyl-1,2-dimethylcyclopentaneethanol

Downstream raw materials:

(1'R,2'R,4E)-1-(1',2'-dimethyl-2'-hydroxymethylcyclopentyl)-6-<2,5-bis(methoxymethoxy)-3-methylpehnyl>-4-methyl-4-hexen-2-yl pivalate

(1'R,2'R,2''E,4E)-6-(5-t-butyldimethylsiloxy-2-hydroxy-3-methylphenyl)-1-<2'-(1'',4''-dihydroxy-4''-methyl-2''-pentynyl)-1',2'-dimethylcyclopentyl>-4-methyl-4-hexen-2-ol

(1'R,2'R,4E)-1-(2'-formyl-1',2'-dimethyl-2'-hydroxymethylcyclopentyl)-6-<2,5-bis(methoxymethoxy)-3-methylpehnyl>-4-methyl-4-hexen-2-yl pivalate

(1'R,2'R,2''E,4E)-6-(5-t-butyldimethylsiloxy-2-hydroxy-3-methylphenyl)-1-<1',2'-dimethyl-2'-(4''-hydroxy-4''-methyl-2''-pentenoyl)cyclopentyl>-4-methyl-4-hexen-2-one

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