[Zn(5-nitroisophthalic acid)(1,2-bis(4-pyridyl)hydrazine)]*ethanol

Base Information

• Chemical Name: [Zn(5-nitroisophthalic acid)(1,2-bis(4-pyridyl)hydrazine)]*ethanol
• CAS No.: 1374979-81-3
• Molecular Formula: C₂H₆O*C₈H₃NO₆*C₁₀H₁₀N₄*Zn
• Molecular Weight: 506.79
• Mol file: 1374979-81-3.mol

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Chemical Property of [Zn(5-nitroisophthalic acid)(1,2-bis(4-pyridyl)hydrazine)]*ethanol

Chemical Property:

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Technology Process of [Zn(5-nitroisophthalic acid)(1,2-bis(4-pyridyl)hydrazine)]*ethanol

There total 1 articles about [Zn(5-nitroisophthalic acid)(1,2-bis(4-pyridyl)hydrazine)]*ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

zinc(II) nitrate hexahydrate + 1,2-bis(5-methylisoxazol-3-yl)hydrazine (2632-99-7) + ethanol (64-17-5) + 5-nitrobenzene-1,3-dicarboxylic acid (618-88-2) → [Zn(5-nitroisophthalic acid)(1,2-bis(4-pyridyl)hydrazine)]*ethanol (1374979-81-3)

Guidance literature:

In ethanol; High Pressure; stirring mixt. of zinc compd., nitroisophthalic acid and azopyridine in ethanol at 60°C for 30 min and then heating at 160°C for 2ds; cooling to room temp. at rate of 5°C/h, decantation, washing withethanol, drying in air for 0.5 h, elem. anal.;

DOI:10.1021/ic300097y

upstream raw materials:

1,2-bis(5-methylisoxazol-3-yl)hydrazine

ethanol

5-nitrobenzene-1,3-dicarboxylic acid