1-methyl-2-phenyl-1H-pyrrolo<2,3-e>pyrido<1,2-b>-as-triazinium tetrafluoroborate

Base Information

Chemical Name:1-methyl-2-phenyl-1H-pyrrolo<2,3-e>pyrido<1,2-b>-as-triazinium tetrafluoroborate
CAS No.:133522-88-0
Molecular Formula:BF₄*C₁₆H₁₃N₄
Molecular Weight:348.111
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-methyl-2-phenyl-1H-pyrrolo<2,3-e>pyrido<1,2-b>-as-triazinium tetrafluoroborate

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Technology Process of 1-methyl-2-phenyl-1H-pyrrolo<2,3-e>pyrido<1,2-b>-as-triazinium tetrafluoroborate

There total 3 articles about 1-methyl-2-phenyl-1H-pyrrolo<2,3-e>pyrido<1,2-b>-as-triazinium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 2-phenylthieno<2,3-e>pyrido<1,2-b>-as-triazinium perchlorate

: 74-89-5
methylamine

: 133522-88-0
1-methyl-2-phenyl-1H-pyrrolo<2,3-e>pyrido<1,2-b>-as-triazinium tetrafluoroborate

Guidance literature:: In acetonitrile;

Reference yield:

: 121232-63-1
2-phenylfuro<2,3-e>pyrido<1,2-b>-as-triazinium perchlorate

: 133522-88-0
1-methyl-2-phenyl-1H-pyrrolo<2,3-e>pyrido<1,2-b>-as-triazinium tetrafluoroborate

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / NaHS / methanol / 0.08 h / Ambient temperature

2: 70 percent / polyphosphoric acid, 70percent perchloric acid / 2 h / 140 - 150 °C

3: 50 percent / acetonitrile

With sodium hydrogensulfide; perchloric acid; PPA; In methanol; acetonitrile;

Reference yield:

: 160684-04-8
2-(benzoylmethyl)-2H-pyrido<1,2-b>-as-triazine-2-thione

: 133522-88-0
1-methyl-2-phenyl-1H-pyrrolo<2,3-e>pyrido<1,2-b>-as-triazinium tetrafluoroborate

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / polyphosphoric acid, 70percent perchloric acid / 2 h / 140 - 150 °C

2: 50 percent / acetonitrile

With perchloric acid; PPA; In acetonitrile;