1-(4',6'-O-diacetyl-2',3'-dideoxy-β-D-erythro-hex-2-enopyranosyl)uracil

Base Information

Chemical Name:1-(4',6'-O-diacetyl-2',3'-dideoxy-β-D-erythro-hex-2-enopyranosyl)uracil
CAS No.:35094-83-8
Molecular Formula:C₁₄H₁₆N₂O₇
Molecular Weight:324.29
Hs Code.:

Synonyms:

Suppliers and Price of 1-(4',6'-O-diacetyl-2',3'-dideoxy-β-D-erythro-hex-2-enopyranosyl)uracil

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4',6'-O-diacetyl-2',3'-dideoxy-β-D-erythro-hex-2-enopyranosyl)uracil

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Technology Process of 1-(4',6'-O-diacetyl-2',3'-dideoxy-β-D-erythro-hex-2-enopyranosyl)uracil

There total 2 articles about 1-(4',6'-O-diacetyl-2',3'-dideoxy-β-D-erythro-hex-2-enopyranosyl)uracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 5707-04-0
Phenylselenyl chloride

: 2873-29-2
D-glucal triacetate

: 160204-60-4
1-(2'-deoxy-2'-phenylselenenyl-3',4',6'-tri-O-acetyl-β-D-gluco-pyranosyl)-uracil

: 1-(2'-deoxy-2'-phenylselenenyl-3',4',6'-tri-O-acetyl-α-D-manno-pyranosyl)-uracil

: 35094-83-8
1-(4',6'-O-diacetyl-2',3'-dideoxy-β-D-erythro-hex-2-enopyranosyl)uracil

Guidance literature:: With silver trifluoromethanesulfonate; In diethyl ether; for 0.5h; Yield given. Yields of byproduct given; Ambient temperature;
DOI:10.1016/S0040-4020(01)89572-7

Reference yield:

: 5707-04-0
Phenylselenyl chloride

: 2873-29-2
D-glucal triacetate

: 160204-60-4
1-(2'-deoxy-2'-phenylselenenyl-3',4',6'-tri-O-acetyl-β-D-gluco-pyranosyl)-uracil

: 1-(2'-deoxy-2'-phenylselenenyl-3',4',6'-tri-O-acetyl-α-D-manno-pyranosyl)-uracil

: 35094-83-8
1-(4',6'-O-diacetyl-2',3'-dideoxy-β-D-erythro-hex-2-enopyranosyl)uracil

Guidance literature:: With silver trifluoromethanesulfonate; 1,3-bis(trimethylsilyl)uracil; In diethyl ether; for 1h; Product distribution; Ambient temperature; effect of various solvents, temperature, reaction time and ratio of reagents in the produduct/yield distribution;
DOI:10.1016/S0040-4020(01)89572-7