2-Cyclohexene-1-ethanesulfonyl chloride

Base Information

Chemical Name:2-Cyclohexene-1-ethanesulfonyl chloride
CAS No.:133216-87-2
Molecular Formula:C₈H₁₃ClO₂S
Molecular Weight:208.709
Hs Code.:
DSSTox Substance ID:DTXSID201281138

Synonyms:2-Cyclohexene-1-ethanesulfonyl chloride;133216-87-2;DTXSID201281138;AKOS006336278

Suppliers and Price of 2-Cyclohexene-1-ethanesulfonyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Cyclohexene-1-ethanesulfonyl chloride

Chemical Property:

XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:208.0324785
Heavy Atom Count:12
Complexity:251

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CC=CC(C1)CCS(=O)(=O)Cl

Technology Process of 2-Cyclohexene-1-ethanesulfonyl chloride

There total 7 articles about 2-Cyclohexene-1-ethanesulfonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₈H₁₃O₃S^(1-)*C₁₆H₃₆N⁽¹⁺⁾

: 133216-87-2
2-(cyclohex-2-en-1-yl)ethane-1-sulfonyl chloride

Guidance literature:: With bis(trichloromethyl) carbonate; N,N-dimethyl-formamide; In dichloromethane; at 0 - 20 ℃; for 1h;
DOI:10.1021/jacs.9b08894

Reference yield:

: 16452-34-9
2-(cyclohex-2-enyl)ethanol

: 133216-87-2
2-(cyclohex-2-en-1-yl)ethane-1-sulfonyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N / CH₂Cl₂ / 0.75 h / 0 °C

2: LiBr / acetone / 1) r.t., 30 min, 2) reflux, overnight

3: sodium sulphite / H₂O / Heating

4: phosphoryl trichloride / 2 h / 130 °C

With triethylamine; lithium bromide; sodium sulfite; trichlorophosphate; In dichloromethane; water; acetone;

Reference yield:

: 79618-45-4
3-(2-bromoethyl)cyclohex-1-ene

: 133216-87-2
2-(cyclohex-2-en-1-yl)ethane-1-sulfonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: sodium sulphite / H₂O / Heating

2: phosphoryl trichloride / 2 h / 130 °C

With sodium sulfite; trichlorophosphate; In water;