trans-4,4'-bis<2-ethyl>azobenzene

Base Information

Chemical Name:trans-4,4'-bis<2-ethyl>azobenzene
CAS No.:99833-21-3
Molecular Formula:C₂₄H₂₈N₄O₈
Molecular Weight:500.508
Hs Code.:

trans-4,4'-bis<2-<bis(carboxymethyl)amino>ethyl>azobenzene

Synonyms:

Suppliers and Price of trans-4,4'-bis<2-ethyl>azobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of trans-4,4'-bis<2-ethyl>azobenzene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of trans-4,4'-bis<2-ethyl>azobenzene

There total 5 articles about trans-4,4'-bis<2-ethyl>azobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 99833-20-2
trans-4,4'-bis(2-chloroethyl)azobenzene

: 142-73-4
iminodiacetic acid

: 99833-21-3
trans-4,4'-bis<2-ethyl>azobenzene

Guidance literature:: With potassium carbonate; In methanol; water; for 21h; Heating;
DOI:10.1246/bcsj.58.2340

Reference yield:

: 100-27-6
2-(4-nitrophenyl)ethanol

: 99833-21-3
trans-4,4'-bis<2-ethyl>azobenzene

Guidance literature:: Multi-step reaction with 4 steps

1: Zn, NaOH / ethanol; H₂O / 1 h / Heating

2: O₂, NaOH / ethanol; H₂O / 2 h

3: 91 percent / thionyl chloride, DMF (drop) / 4 h

4: 35 percent / K₂CO₃ / methanol; H₂O / 21 h / Heating

With sodium hydroxide; thionyl chloride; oxygen; potassium carbonate; N,N-dimethyl-formamide; zinc; In methanol; ethanol; water;
DOI:10.1246/bcsj.58.2340

Reference yield:

: 2-(4-{N'-[4-(2-Hydroxy-ethyl)-phenyl]-hydrazino}-phenyl)-ethanol

: 99833-21-3
trans-4,4'-bis<2-ethyl>azobenzene

Guidance literature:: Multi-step reaction with 3 steps

1: O₂, NaOH / ethanol; H₂O / 2 h

2: 91 percent / thionyl chloride, DMF (drop) / 4 h

3: 35 percent / K₂CO₃ / methanol; H₂O / 21 h / Heating

With sodium hydroxide; thionyl chloride; oxygen; potassium carbonate; N,N-dimethyl-formamide; In methanol; ethanol; water;
DOI:10.1246/bcsj.58.2340