1,1,3,3-tetraphenyldistibaselenane

Base Information

Chemical Name:1,1,3,3-tetraphenyldistibaselenane
CAS No.:95837-59-5
Molecular Formula:C₂₄H₂₀Sb₂Se
Molecular Weight:630.883
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1,3,3-tetraphenyldistibaselenane

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Technology Process of 1,1,3,3-tetraphenyldistibaselenane

There total 7 articles about 1,1,3,3-tetraphenyldistibaselenane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: selenium

: 2654-44-6
tetraphenyldistibane

: 95837-59-5
1,1,3,3-tetraphenyldistibaselenane

Guidance literature:: In carbon disulfide; a mixt. of black Se powder and Ph4Sb2 was stirred in CS2 under reflux for 4 h under Ar atmosphere; soln. was filtered, filtrate evapd., residue recrystd. from 1:1 MeOH-C6H6; elem. anal.;
DOI:10.1016/0022-328X(84)80706-8

Reference yield: 66.0%

: sodium selenide

: 2629-47-2
diphenylantimony(III) chloride

: 95837-59-5
1,1,3,3-tetraphenyldistibaselenane

Guidance literature:: In not given; Sb-compound was added to a suspn. of sodium selenide, the mixt. was stirred at 22°C for 4 h; filtered, evapd.;
DOI:10.1002/hlca.200690070

Reference yield: 1.0%

: 110-89-4
piperidine

: [(4-methylbenzoyl)seleno]diphenylantimony

: 95837-59-5
1,1,3,3-tetraphenyldistibaselenane

: 895166-06-0
piperidinium diphenylstibinoselenoite

Guidance literature:: In diethyl ether; byproducts: N-(4-methylbenzoyl)piperidine; to a suspn. of Sb-compound in diethyl ether was added a soln. of piperidine in diethyl ether at room temp., the mixt. was stirred at 0°C for 1 h; evapd., chromy. on silica gel (diethyl ether);
DOI:10.1002/hlca.200690070