2-[(N,N-dimethylaminomethyl)phenyl]diphenylstannylfluoride

Base Information

Chemical Name:2-[(N,N-dimethylaminomethyl)phenyl]diphenylstannylfluoride
CAS No.:712351-41-2
Molecular Formula:C₂₁H₂₂FNSn
Molecular Weight:426.121
Hs Code.:

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Chemical Property of 2-[(N,N-dimethylaminomethyl)phenyl]diphenylstannylfluoride

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Technology Process of 2-[(N,N-dimethylaminomethyl)phenyl]diphenylstannylfluoride

There total 2 articles about 2-[(N,N-dimethylaminomethyl)phenyl]diphenylstannylfluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 7789-23-3
potassium fluoride

: 342371-85-1
C,N-[2-(dimethylaminomethyl)phenyl]diphenyltin(IV) chloride

: 712351-41-2
2-[(N,N-dimethylaminomethyl)phenyl]diphenylstannylfluoride

Guidance literature:: In methanol; dichloromethane; water; byproducts: KCl; (Ar), CH2Cl2 added to suspn. of Sn complex in CH3OH, treated with KF in H2O, stirred for 3 h at room temp.; water soln. washed twice (CH2Cl2), organic layers dried (Na2SO4), filtered, evapd.(vac.), recrystd.(CH2Cl2/n-hexane), elem. anal.;
DOI:10.1002/ejic.200501018

Reference yield: 70.0%

: 7789-23-3
potassium fluoride

: 342371-85-1
[2-(N,N-dimethylaminomethyl)phenyl]diphenyltin(IV) chloride

: 712351-41-2
2-[(N,N-dimethylaminomethyl)phenyl]diphenylstannylfluoride

Guidance literature:: In diethyl ether; water; under Ar atm. to soln. to soln. triorganotin chloride in Et2O KF in water was added and stirred for 2 + 2 days; org. layer was dried over Na2SO4, filtered, and evapd. to dryness, residue was washed with cold pentane; elem. anal.;
DOI:10.1021/om049912q

Reference yield:

: 1271-19-8
bis(cyclopentadienyl)titanium dichloride

: 712351-41-2
2-[(N,N-dimethylaminomethyl)phenyl]diphenylstannylfluoride

: 309-89-7
titanocene difluoride

: 342371-85-1
[2-(N,N-dimethylaminomethyl)phenyl]diphenyltin(IV) chloride

Guidance literature:: In dichloromethane; under Ar atm. Cp2TiCl2 was added to soln. triorganotin fluoride in CH2Cl2 and stirred for 3 h at 35°C; solvent was evapd. in vacuo - products were not separated;
DOI:10.1021/om049912q