1-ferrocenyl-3-phenylpropane-1,3-dione

Base Information

Chemical Name:1-ferrocenyl-3-phenylpropane-1,3-dione
CAS No.:162823-13-4
Molecular Formula:C₁₉H₁₆FeO₂
Molecular Weight:332.182
Hs Code.:

Synonyms:

Suppliers and Price of 1-ferrocenyl-3-phenylpropane-1,3-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-ferrocenyl-3-phenylpropane-1,3-dione

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-ferrocenyl-3-phenylpropane-1,3-dione

There total 2 articles about 1-ferrocenyl-3-phenylpropane-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 93-58-3,5705-52-2,80226-58-0
benzoic acid methyl ester

: 1271-55-2
acetylferrocene

: 3-methyl-1,3-bis(ferrocenyl)propen-1-one

: 162823-13-4
1-ferrocenyl-3-phenylpropane-1,3-dione

Guidance literature:: With diisopropylamine; n-BuLi; In tetrahydrofuran; hexane; (Schlenk conditions); addn. of n-BuLi in hexane to ice-cold diisopropylamine in THF,, addn. to acetylferrocene in THF, stirring (room temp., 20 min), addn. of methyl benzoate in THF, stirring (4 h); shaking with aq. HCl, extn. (Et2O), washing (H2O), drying (MgSO4), evapn. to dryness (reduced pressure), flash chromy. (SiO2; Et2O/hexane); elem. anal.;
DOI:10.1039/a802398k

Reference yield:

: [Cu((C₅H₅)Fe(C₅H₄COCHC(O)C₆H₅))2]

: 162823-13-4
1-ferrocenyl-3-phenylpropane-1,3-dione

Guidance literature:: With aq. HCl; In chloroform; water; dissoln. of the Cu complex in CHCl3, shaking with aq. HCl; washing (H2O), evapn. to dryness (reduced pressure);
DOI:10.1039/a802398k

Reference yield: 77.0%

: 12092-47-6
di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium

: 162823-13-4
1-ferrocenyl-3-phenylpropane-1,3-dione

: 213037-38-8
[Rh(C₈H₁₂)(C₅H₅)Fe(C₅H₄COCHC(O)C₆H₅)]

Guidance literature:: In N,N-dimethyl-formamide; stirring (5 min); addn. of H2O, filtration, dissoln. (Et2O), washing (H2O), drying (MgSO4), evapn. to dryness, flash chromy. (SiO2; Et2O/hexane);
DOI:10.1039/a802398k