1-Phenylsulfonyl-3-thiazol-2-ylindole

Base Information

Chemical Name:1-Phenylsulfonyl-3-thiazol-2-ylindole
CAS No.:154787-38-9
Molecular Formula:C₁₇H₁₂N₂O₂S₂
Molecular Weight:340.426
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Phenylsulfonyl-3-thiazol-2-ylindole

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Technology Process of 1-Phenylsulfonyl-3-thiazol-2-ylindole

There total 3 articles about 1-Phenylsulfonyl-3-thiazol-2-ylindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 120-72-9
indole

: 154787-38-9
1-Phenylsulfonyl-3-thiazol-2-ylindole

Guidance literature:: Multi-step reaction with 3 steps

1: KOH, I₂ / dimethylformamide / 0.17 h / Ambient temperature

2: 50percent aq. NaOH, tetrabutylammonium bromide / benzene / 2 h / Ambient temperature

3: 1.) Zn / 2.) Pd(PPh₃)4 / 1.) THF, r.t., 2 h, 2.) THF, r.t., 18 h

With potassium hydroxide; sodium hydroxide; tetrabutylammomium bromide; iodine; zinc; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; benzene;
DOI:10.1039/p19960001927

Reference yield:

: 26340-47-6
3-Iodo-1H-indole

: 154787-38-9
1-Phenylsulfonyl-3-thiazol-2-ylindole

Guidance literature:: Multi-step reaction with 2 steps

1: 50percent aq. NaOH, tetrabutylammonium bromide / benzene / 2 h / Ambient temperature

2: 1.) Zn / 2.) Pd(PPh₃)4 / 1.) THF, r.t., 2 h, 2.) THF, r.t., 18 h

With sodium hydroxide; tetrabutylammomium bromide; zinc; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In benzene;
DOI:10.1039/p19960001927

Reference yield:

: 3034-54-6
2-iodo-1,3-thiazole

: 80360-14-1
3-iodo-1-phenylsulfonyl-1H-indole

: 154787-38-9
1-Phenylsulfonyl-3-thiazol-2-ylindole

Guidance literature:: With zinc; tetrakis(triphenylphosphine) palladium⁽⁰⁾; Yield given. Multistep reaction; 1.) THF, r.t., 2 h; 2.) THF, r.t., 18 h;
DOI:10.1016/S0040-4039(00)73824-X