bis-iodo{N-(2,3,5,6-tetrafluorophenyl)ethane-1,2-diamine}platinum(II)

Base Information

Chemical Name:bis-iodo{N-(2,3,5,6-tetrafluorophenyl)ethane-1,2-diamine}platinum(II)
CAS No.:135389-34-3
Molecular Formula:C₈H₈F₄I₂N₂Pt
Molecular Weight:657.048
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis-iodo{N-(2,3,5,6-tetrafluorophenyl)ethane-1,2-diamine}platinum(II)

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Technology Process of bis-iodo{N-(2,3,5,6-tetrafluorophenyl)ethane-1,2-diamine}platinum(II)

There total 1 articles about bis-iodo{N-(2,3,5,6-tetrafluorophenyl)ethane-1,2-diamine}platinum(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: 10025-99-7
potassium tetrachloroplatinate(II)

: 135497-81-3
N-(2,3,5,6-tetrafluorophenyl)ethane-1,2-diamine

: 135389-34-3
bis-iodo{N-(2,3,5,6-tetrafluorophenyl)ethane-1,2-diamine}platinum(II)

Guidance literature:: With potassium iodide; In ethanol; water; K2PtCl4 and KI stirred in water with heating for 0.5 h, HC6F4NHCH2CH2NH2 in ethanol added, stirred overnight; washed with ethanol and ether, recrystd. from acetone-petrol, refluxed in ether for 2 h, elem. anal.;
DOI:10.1016/S0277-5387(00)83764-X

Reference yield: 30.0%

: 135389-34-3
bis-iodo{N-(2,3,5,6-tetrafluorophenyl)ethane-1,2-diamine}platinum(II)

: 363-72-4
Pentafluorobenzene

: 92181-58-3
{N,N'-bis(2,3,5,6-tetrafluorophenyl)ethane-1,2-diaminato^(2-)}dipyridineplatinum(II)

Guidance literature:: With TlO₂CC₆F₄H; In pyridine; byproducts: CO2; (N2), heated at 105-107°C with stirring for 25 min; evapd. to dryness in vacuo, washed with petrol, extracted (acetone), filtered, evapd., recrystd. from ether-petrol, IR, mass spectra;
DOI:10.1016/S0277-5387(00)83764-X

Reference yield: 15.0%

: 135389-34-3
bis-iodo{N-(2,3,5,6-tetrafluorophenyl)ethane-1,2-diamine}platinum(II)

: 344-04-7
bromopentafluorobenzene

: {N-(4-bromo-2,3,5,6-tetrafluorophenyl)-N'-(2,3,5,6-tetrafluorophenyl)ethane-1,2-diaminato^(2-)}dipyridineplatinum(II)*0.5Et₂O

Guidance literature:: With TlO₂CC₆F₄H; In pyridine; byproducts: CO2; (N2), heated at 105-110°C with stirring for 22 min; evapd. to dryness in vacuo, washed with petrol, extracted (acetone), filtered, evapd., recrystd. from ether-petrol, elem. anal.;
DOI:10.1016/S0277-5387(00)83764-X