[tBuC(N(Dipp))2-η2]BiCl2

Base Information

• Chemical Name: [tBuC(N(Dipp))2-η2]BiCl2
• CAS No.: 1208986-14-4
• Molecular Formula: C₂₉H₄₃BiCl₂N₂
• Molecular Weight: 699.56

Synonyms:

Chemical Property of [tBuC(N(Dipp))2-η2]BiCl2

Chemical Property:

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Technology Process of [tBuC(N(Dipp))2-η2]BiCl2

There total 1 articles about [tBuC(N(Dipp))2-η2]BiCl2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

lithium N,N'-bis(2,6-di-isopropylphenyl)tert-butylamidinate + bismuth(III) chloride (7787-60-2) → [tBuC(N(Dipp))2-η2]BiCl2 (1208986-14-4)

Guidance literature:

In diethyl ether; under Ar using standard Schlenk techniques or in glove box; solid tBuC(N(2,6-diisopropylphenyl))2 (1 mol) added within 1 h to soln. BiCl3 (1 mol) in Et2O at -78°C; stirred for 1 h; warmed to ambient temp. overperiod of 6 h; ppt. filtered off; extd. (twice, CHCl3); solvent evapd. (vac.); elem. anal.; XRD;

DOI:10.1002/ejic.200900233

upstream raw materials:

bismuth(III) chloride

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