tetraphenylphosphonium [p-tert-butyl-calix[4]arene tetrahydroxylato oxovanadate(V)] dichloromethane adduct (1/1)

Base Information

Chemical Name:tetraphenylphosphonium [p-tert-butyl-calix[4]arene tetrahydroxylato oxovanadate(V)] dichloromethane adduct (1/1)
CAS No.:910629-04-8
Molecular Formula:CH₂Cl₂*C₂₄H₂₀P*C₄₄H₅₂O₅V
Molecular Weight:1136.16
Hs Code.:

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Chemical Property of tetraphenylphosphonium [p-tert-butyl-calix[4]arene tetrahydroxylato oxovanadate(V)] dichloromethane adduct (1/1)

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Technology Process of tetraphenylphosphonium [p-tert-butyl-calix[4]arene tetrahydroxylato oxovanadate(V)] dichloromethane adduct (1/1)

There total 1 articles about tetraphenylphosphonium [p-tert-butyl-calix[4]arene tetrahydroxylato oxovanadate(V)] dichloromethane adduct (1/1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 37017-97-3
tetraphenylphosphonium dichlorodioxovanadate(V)

: 75-09-2
dichloromethane

: tetralithiated 4-tert-butylcalix[4]arene

: 910629-04-8
tetraphenylphosphonium [p-tert-butyl-calix[4]arene tetrahydroxylato oxovanadate(V)] dichloromethane adduct (1/1)

Guidance literature:: In toluene; byproducts: LiCl, Li2O; (Ar); a soln. of Li salt added to V compd., refluxed for 20 h; allowed to cool to room temp., evapd., washed (MeOH), dried, dissolved in CH2Cl2, pptd. (n-hexane); elem. anal.;
DOI:10.1021/ic061106j