C₂₈H₄₇NO₆Si

Base Information Edit

Chemical Name:C₂₈H₄₇NO₆Si
CAS No.:1568951-23-4
Molecular Formula:C₂₈H₄₇NO₆Si
Molecular Weight:521.77
Hs Code.:
Mol file:1568951-23-4.mol

C<sub>28</sub>H<sub>47</sub>NO<sub>6</sub>Si

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Chemical Property of C₂₈H₄₇NO₆Si Edit

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Technology Process of C₂₈H₄₇NO₆Si

There total 12 articles about C₂₈H₄₇NO₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1414941-34-6
C₂₈H₄₉NO₆Si

: 1568951-23-4
C₂₈H₄₇NO₆Si

Guidance literature:: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dichloromethane; dimethyl sulfoxide; at 20 ℃; for 4.5h;
DOI:10.1002/chem.201302197

Reference yield:

: 446264-36-4
3-[(4-methoxyphenyl)methoxy]-2,2-dimethyl-propan-1-ol

: 1568951-23-4
C₂₈H₄₇NO₆Si

Guidance literature:: Multi-step reaction with 6 steps

1: bis(1,5-cyclooctadiene)diiridium(I) dichloride; caesium carbonate; (S)-(-)-5,5'-dichloro-6,6'-dimethoxy-2,2'-bis(diphenylphosphino)-1,1'-biphenyl; 4-chloro-3-nitrobenzoate / tetrahydrofuran / Inert atmosphere

2: 2,6-dimethylpyridine / dichloromethane / 1 h / -78 °C / Inert atmosphere

3: Sudan III; ozone; triphenylphosphine / dichloromethane / 2 h / -78 - 20 °C

4: sodium chlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol / 1.5 h / 20 °C / Inert atmosphere

5: triethylamine / tetrahydrofuran / 20 °C

6: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dichloromethane; dimethyl sulfoxide / 4.5 h / 20 °C

With 2,6-dimethylpyridine; sodium dihydrogenphosphate; (S)-(-)-5,5'-dichloro-6,6'-dimethoxy-2,2'-bis(diphenylphosphino)-1,1'-biphenyl; bis(1,5-cyclooctadiene)diiridium(I) dichloride; sodium chlorite; caesium carbonate; ozone; triethylamine; triphenylphosphine; 4-chloro-3-nitrobenzoate; Sudan III; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; tert-butyl alcohol;
DOI:10.1002/chem.201302197

Reference yield:

: 869062-10-2
1-(4-methoxy-benzyloxy)-2,2-dimethyl-hex-5-en-3-ol

: 1568951-23-4
C₂₈H₄₇NO₆Si

Guidance literature:: Multi-step reaction with 5 steps

1: 2,6-dimethylpyridine / dichloromethane / 1 h / -78 °C / Inert atmosphere

2: Sudan III; ozone; triphenylphosphine / dichloromethane / 2 h / -78 - 20 °C

3: sodium chlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol / 1.5 h / 20 °C / Inert atmosphere

4: triethylamine / tetrahydrofuran / 20 °C

5: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dichloromethane; dimethyl sulfoxide / 4.5 h / 20 °C

With 2,6-dimethylpyridine; sodium dihydrogenphosphate; sodium chlorite; ozone; triethylamine; triphenylphosphine; Sudan III; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; tert-butyl alcohol;
DOI:10.1002/chem.201302197