Mg2(μ-Cl)2(tetrahydrofuran)[Ph(pyrazol-1-yl)B(μ-N(Me))(μ-pyrazol-1-yl)B(pyrazol-1-yl)Ph]2*pentane

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Chemical Name:Mg2(μ-Cl)2(tetrahydrofuran)[Ph(pyrazol-1-yl)B(μ-N(Me))(μ-pyrazol-1-yl)B(pyrazol-1-yl)Ph]2*pentane
CAS No.:1220508-55-3
Molecular Formula:C₅H₁₂*C₄₈H₅₂B₄Cl₂Mg₂N₁₄O
Molecular Weight:1075.94
Hs Code.:

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Chemical Property of Mg2(μ-Cl)2(tetrahydrofuran)[Ph(pyrazol-1-yl)B(μ-N(Me))(μ-pyrazol-1-yl)B(pyrazol-1-yl)Ph]2*pentane

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Technology Process of Mg2(μ-Cl)2(tetrahydrofuran)[Ph(pyrazol-1-yl)B(μ-N(Me))(μ-pyrazol-1-yl)B(pyrazol-1-yl)Ph]2*pentane

There total 1 articles about Mg2(μ-Cl)2(tetrahydrofuran)[Ph(pyrazol-1-yl)B(μ-N(Me))(μ-pyrazol-1-yl)B(pyrazol-1-yl)Ph]2*pentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: [Ph(pyrazol-1-yl)B(μ-NH(Me))(μ-pyrazol-1-yl)B(pyrazol-1-yl)Ph]

: 676-58-4
methylmagnesium chloride

: 109-66-0,8031-35-4,9078-70-0
pentane

: MgCl(tetrahydrofuran)(x)[Ph(pyrazol-1-yl)B(μ-N(Me))(μ-pyrazol-1-yl)B(pyrazol-1-yl)Ph]

: 1220508-55-3
Mg2(μ-Cl)2(tetrahydrofuran)[Ph(pyrazol-1-yl)B(μ-N(Me))(μ-pyrazol-1-yl)B(pyrazol-1-yl)Ph]2*pentane

Guidance literature:: In tetrahydrofuran; under N2 atm. using Schlenk techniques; stirred soln. of borate ligand in THF was treated at -78°C with soln. of MeMgCl in THF; mixt. allowed to warm to room temp.; stirred overnight; soln. concd. (vac.); layered with pentane; crystals are formed; mother liq. decanted; dried (vac.);
DOI:10.1021/ic100104t