bis(p-tolylimido)-bis(diethyl dithiophosphato)-(μ-acetato)-dimolybdenum(V)-(μ-S)-(μ-SOBn)

Base Information

Chemical Name:bis(p-tolylimido)-bis(diethyl dithiophosphato)-(μ-acetato)-dimolybdenum(V)-(μ-S)-(μ-SOBn)
CAS No.:1159216-45-1
Molecular Formula:C₃₁H₄₄Mo₂N₂O₇P₂S₆
Molecular Weight:1002.92
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(p-tolylimido)-bis(diethyl dithiophosphato)-(μ-acetato)-dimolybdenum(V)-(μ-S)-(μ-SOBn)

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Technology Process of bis(p-tolylimido)-bis(diethyl dithiophosphato)-(μ-acetato)-dimolybdenum(V)-(μ-S)-(μ-SOBn)

There total 1 articles about bis(p-tolylimido)-bis(diethyl dithiophosphato)-(μ-acetato)-dimolybdenum(V)-(μ-S)-(μ-SOBn) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 176799-53-4,176897-18-0,176897-19-1,176897-20-4
[Mo2(N-p-tolyl)2(S2P(OEt)2)2(μ-SCH2Ph)(μ-SO)]

: 100-39-0
benzyl bromide

: 1159216-45-1
bis(p-tolylimido)-bis(diethyl dithiophosphato)-(μ-acetato)-dimolybdenum(V)-(μ-S)-(μ-SOBn)

Guidance literature:: In acetone; to soln. Mo complex in acetone C6H5CH2Br was added, stirred for 2.9 h; EtOH/H2O (1:1) was added, ppt. was filtered and washed with EtOH/H2O (1:1), suction-dried - mixt. invertomer;
DOI:10.1021/ic9002093