Au(NH₃)(P(C₆H₅)3)⁽¹⁺⁾*ClO₄^(1-)=[Au(NH₃)(P(C₆H₅)3)]ClO₄

Base Information

• Chemical Name: Au(NH₃)(P(C₆H₅)3)⁽¹⁺⁾*ClO₄^(1-)=[Au(NH₃)(P(C₆H₅)3)]ClO₄
• CAS No.: 194206-63-8
• Molecular Formula: C₁₈H₁₈AuNP*ClO₄
• Molecular Weight: 575.738

Synonyms:

Chemical Property of Au(NH₃)(P(C₆H₅)3)⁽¹⁺⁾*ClO₄^(1-)=[Au(NH₃)(P(C₆H₅)3)]ClO₄

Chemical Property:

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Technology Process of Au(NH₃)(P(C₆H₅)3)⁽¹⁺⁾*ClO₄^(1-)=[Au(NH₃)(P(C₆H₅)3)]ClO₄

There total 1 articles about Au(NH₃)(P(C₆H₅)3)⁽¹⁺⁾*ClO₄^(1-)=[Au(NH₃)(P(C₆H₅)3)]ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

ammonium perchlorate (7790-98-9) + 3-[(triphenylphosphine)gold]pentane-2,4-dione → Au(NH3)(P(C6H5)3)(1+)*ClO4(1-)=[Au(NH3)(P(C6H5)3)]ClO4 (194206-63-8)

Guidance literature:

In tetrahydrofuran; byproducts: acetylacetone; dropwise addn. of soln. of Au-complex to suspn. of slight stoich. excessNH4ClO4, stirring at room temp. for 1 h; filtration (Celite), concn., pptn. on Et2O addn., collection (filtration), washing (Et2O), recrystn. (THF and Et2O), washing (pentane); elem. anal.;

DOI:10.1021/ic970225j

Reference yield: 78.0%

3-[(triphenylphosphine)gold]pentane-2,4-dione + Au(NH3)(P(C6H5)3)(1+)*ClO4(1-)=[Au(NH3)(P(C6H5)3)]ClO4 (194206-63-8) → [(AuPPh3)2(μ-NH2)]ClO4 (194206-77-4)

Guidance literature:

In dichloromethane; byproducts: acetylacetone; N2-atmosphere; stirring at room temp. for 10 min; concn., pptn. on Et2O addn., recrystn. (CH2Cl2 and Et2O); elem. anal.;

DOI:10.1021/ic970225j

Reference yield:

3-[(triphenylphosphine)gold]pentane-2,4-dione + Au(NH3)(P(C6H5)3)(1+)*ClO4(1-)=[Au(NH3)(P(C6H5)3)]ClO4 (194206-63-8) + water (7732-18-5) → [(AuPPh3)3(μ-O)]ClO4 + [(AuPPh3)2(μ-NH2)]ClO4 (194206-77-4)

Guidance literature:

In dichloromethane; byproducts: acetylacetone; N2-atmosphere; stirring at room temp. (source of water unclear);

DOI:10.1021/ic970225j

upstream raw materials:

ammonium perchlorate

Downstream raw materials:

[(AuPPh3)2(μ-NH2)]ClO4

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