Technology Process of bis(salicylidene-benzoyl hydrazido)mercury(II)
There total 2 articles about bis(salicylidene-benzoyl hydrazido)mercury(II) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium hydroxide;
In
ethanol; acetone;
a solution of the metal chloride in ethanol (50%) was mixed with the organic ligand dissolved in acetone; KOH (1%) was added dropwise to pH 3,5; digested for about 1 h; further digested for 2 h; filtered; washed withethanol, acetone and ether; dried under vacuum; elem. anal.;
DOI:10.1016/0022-1902(80)80145-X
- Guidance literature:
-
With
acetic acid;
In
ethanol;
refluxing a soln. of Hg(CH3COO)2 in ethanol (addn. of a few drops of CH3COOH) and ligand in ethanol for 30 min, treating with water, digesting on a steam-bath for 1 h, pptn.; filtn., washing with ethanol, drying in vacuo over silica gel, elem. anal.;
