ReO₂(N-o-methoxyphenyl-N'-2-mercaptoethylpiperazine)PPh₃*MeOH

Base Information

• Chemical Name: ReO₂(N-o-methoxyphenyl-N'-2-mercaptoethylpiperazine)PPh₃*MeOH
• CAS No.: 374631-84-2
• Molecular Formula: CH₄O*C₃₁H₃₄N₂O₃PReS
• Molecular Weight: 763.911
• Mol file: 374631-84-2.mol

Synonyms:

Chemical Property of ReO₂(N-o-methoxyphenyl-N'-2-mercaptoethylpiperazine)PPh₃*MeOH

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of ReO₂(N-o-methoxyphenyl-N'-2-mercaptoethylpiperazine)PPh₃*MeOH

There total 1 articles about ReO₂(N-o-methoxyphenyl-N'-2-mercaptoethylpiperazine)PPh₃*MeOH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

methanol (67-56-1) + [ReOCl3(PPh3)2] + N-o-methoxyphenyl-N'-2-mercaptoethylpiperazine (350229-20-8) → ReO2(N-o-methoxyphenyl-N'-2-mercaptoethylpiperazine)PPh3*MeOH (374631-84-2)

Guidance literature:

With AcONa; In methanol; to soln. of AcONa in MeOH, Re-complex and ligand were added under stirring, refluxed; CH2Cl2 was added, washed with H2O, dried, concd., column chromy. on silica gel with CH2Cl2, slow evapd. from CH2Cl2-MeOH; elem. anal.;

DOI:10.1016/S0020-1693(01)00474-1

upstream raw materials:

methanol

N-o-methoxyphenyl-N'-2-mercaptoethylpiperazine