11-{3-[1-(4-acetoxyphenyl)-2,2,2-trifluoroethoxysulfonyl]propyl}-3,4,8,9,10,11-hexahydro-2H-13-oxa-6,11-diaza-1-azonia-pentacene trifluoroacetate

Base Information

Chemical Name:11-{3-[1-(4-acetoxyphenyl)-2,2,2-trifluoroethoxysulfonyl]propyl}-3,4,8,9,10,11-hexahydro-2H-13-oxa-6,11-diaza-1-azonia-pentacene trifluoroacetate
CAS No.:1345614-74-5
Molecular Formula:C₂F₃O₂*C₃₃H₃₅F₃N₃O₆S
Molecular Weight:771.735
Hs Code.:

11-{3-[1-(4-acetoxyphenyl)-2,2,2-trifluoroethoxysulfonyl]propyl}-3,4,8,9,10,11-hexahydro-2H-13-oxa-6,11-diaza-1-azonia-pentacene trifluoroacetate

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Chemical Property of 11-{3-[1-(4-acetoxyphenyl)-2,2,2-trifluoroethoxysulfonyl]propyl}-3,4,8,9,10,11-hexahydro-2H-13-oxa-6,11-diaza-1-azonia-pentacene trifluoroacetate

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Technology Process of 11-{3-[1-(4-acetoxyphenyl)-2,2,2-trifluoroethoxysulfonyl]propyl}-3,4,8,9,10,11-hexahydro-2H-13-oxa-6,11-diaza-1-azonia-pentacene trifluoroacetate

There total 8 articles about 11-{3-[1-(4-acetoxyphenyl)-2,2,2-trifluoroethoxysulfonyl]propyl}-3,4,8,9,10,11-hexahydro-2H-13-oxa-6,11-diaza-1-azonia-pentacene trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19500-61-9
7-methoxy-1,2,3,4-tetrahydroquinoline

: 1345614-74-5
11-{3-[1-(4-acetoxyphenyl)-2,2,2-trifluoroethoxysulfonyl]propyl}-3,4,8,9,10,11-hexahydro-2H-13-oxa-6,11-diaza-1-azonia-pentacene trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 65 °C

2: sulfuric acid / methanol; water / 1 h / 20 °C

3: acetic acid / 1.17 h / 80 °C

With sulfuric acid; potassium carbonate; In methanol; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/ol202619f

Reference yield:

: 1345614-61-0
acetic acid 4-[1-(3-chloropropane-1-sulfonyloxy)-2,2,2-trifluoroethyl]phenyl ester

: 1345614-74-5
11-{3-[1-(4-acetoxyphenyl)-2,2,2-trifluoroethoxysulfonyl]propyl}-3,4,8,9,10,11-hexahydro-2H-13-oxa-6,11-diaza-1-azonia-pentacene trifluoroacetate

Guidance literature:: Multi-step reaction with 4 steps

1: sodium iodide / acetone / 17 h / Reflux

2: potassium carbonate / N,N-dimethyl-formamide / 65 °C

3: sulfuric acid / methanol; water / 1 h / 20 °C

4: acetic acid / 1.17 h / 80 °C

With sulfuric acid; potassium carbonate; sodium iodide; In methanol; water; acetic acid; N,N-dimethyl-formamide; acetone;
DOI:10.1021/ol202619f

Reference yield:

: 1279691-41-6
acetic acid 4-(2,2,2-trifluoro-1-hydroxyethyl)phenyl ester

: 1345614-74-5
11-{3-[1-(4-acetoxyphenyl)-2,2,2-trifluoroethoxysulfonyl]propyl}-3,4,8,9,10,11-hexahydro-2H-13-oxa-6,11-diaza-1-azonia-pentacene trifluoroacetate

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / dichloromethane / 1 h / 0 °C

2: sodium iodide / acetone / 17 h / Reflux

3: potassium carbonate / N,N-dimethyl-formamide / 65 °C

4: sulfuric acid / methanol; water / 1 h / 20 °C

5: acetic acid / 1.17 h / 80 °C

With sulfuric acid; potassium carbonate; triethylamine; sodium iodide; In methanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; acetone;
DOI:10.1021/ol202619f