acetic acid 4-[1-(3-chloropropane-1-sulfonyloxy)-2,2,2-trifluoroethyl]phenyl ester

Base Information

Chemical Name:acetic acid 4-[1-(3-chloropropane-1-sulfonyloxy)-2,2,2-trifluoroethyl]phenyl ester
CAS No.:1345614-61-0
Molecular Formula:C₁₃H₁₄ClF₃O₅S
Molecular Weight:374.765
Hs Code.:

Synonyms:acetic acid 4-[1-(3-chloropropane-1-sulfonyloxy)-2,2,2-trifluoroethyl]phenyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of acetic acid 4-[1-(3-chloropropane-1-sulfonyloxy)-2,2,2-trifluoroethyl]phenyl ester

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Technology Process of acetic acid 4-[1-(3-chloropropane-1-sulfonyloxy)-2,2,2-trifluoroethyl]phenyl ester

There total 1 articles about acetic acid 4-[1-(3-chloropropane-1-sulfonyloxy)-2,2,2-trifluoroethyl]phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1633-82-5
3-chloro-n-propanesulfonyl chloride

: 1279691-41-6
acetic acid 4-(2,2,2-trifluoro-1-hydroxyethyl)phenyl ester

: 1345614-61-0
acetic acid 4-[1-(3-chloropropane-1-sulfonyloxy)-2,2,2-trifluoroethyl]phenyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1021/ol202619f

Reference yield: 97.0%

: 1345614-61-0
acetic acid 4-[1-(3-chloropropane-1-sulfonyloxy)-2,2,2-trifluoroethyl]phenyl ester

: 1345614-63-2
acetic acid 4-[1-(3-iodopropane-1-sulfonyloxy)-2,2,2-trifluoroethyl]phenyl ester

Guidance literature:: With sodium iodide; In acetone; for 17h; Reflux;
DOI:10.1021/ol202619f

Reference yield:

: 1345614-61-0
acetic acid 4-[1-(3-chloropropane-1-sulfonyloxy)-2,2,2-trifluoroethyl]phenyl ester

: 1345614-80-3
1,11-bis{3-[1-(4-acetoxyphenyl)-2,2,2-trifluoroethoxysulfonyl]propyl}-3,4,8,9,10,11-hexahydro-2H-13-oxa-6,11-diaza-1-azonia-pentacene tetrafluoroborate

Guidance literature:: Multi-step reaction with 4 steps

1: sodium iodide / acetone / 17 h / Reflux

2: potassium carbonate / N,N-dimethyl-formamide / 65 °C

3: sulfuric acid / methanol; water / 1 h / 20 °C

4: acetic acid / 2.5 h / 80 °C

With sulfuric acid; potassium carbonate; sodium iodide; In methanol; water; acetic acid; N,N-dimethyl-formamide; acetone;
DOI:10.1021/ol202619f