C₃₂H₂₈ClFN₄O₉S

Base Information

Chemical Name:C₃₂H₂₈ClFN₄O₉S
CAS No.:1417792-23-4
Molecular Formula:C₃₂H₂₈ClFN₄O₉S
Molecular Weight:699.113
Hs Code.:

C<sub>32</sub>H<sub>28</sub>ClFN<sub>4</sub>O<sub>9</sub>S

Synonyms:

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Chemical Property of C₃₂H₂₈ClFN₄O₉S

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Technology Process of C₃₂H₂₈ClFN₄O₉S

There total 12 articles about C₃₂H₂₈ClFN₄O₉S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 1417792-49-4
C₃₅H₃₄ClFN₄O₉S

: 1417792-23-4
C₃₂H₂₈ClFN₄O₉S

Guidance literature:: With water; potassium carbonate; In methanol; at 90 ℃; for 0.25h;
DOI:10.1021/jm3014844

Reference yield:

: 73781-91-6
6-Chloronicotinic acid methyl ester

: 1417792-23-4
C₃₂H₂₈ClFN₄O₉S

Guidance literature:: Multi-step reaction with 6 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,4-dioxane / 80 °C / Inert atmosphere

2: potassium carbonate / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3: trifluoroacetic acid / 20 °C

4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C

5: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 °C

6: potassium carbonate; water / methanol / 0.25 h / 90 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; di-isopropyl azodicarboxylate; water; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; methanol; N,N-dimethyl-formamide; 1: |Suzuki Coupling;
DOI:10.1021/jm3014844

Reference yield:

: 1089280-66-9
1-chloro-2-fluoro-4-methoxy-5-nitrobenzene

: 1417792-23-4
C₃₂H₂₈ClFN₄O₉S

Guidance literature:: Multi-step reaction with 5 steps

1: potassium hydroxide / water; dimethyl sulfoxide / 1 h / 100 °C

2: zinc; ammonium chloride / water; acetone / 0.5 h / 20 °C

3: dicyclohexyl-carbodiimide; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C

4: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 °C

5: potassium carbonate; water / methanol / 0.25 h / 90 °C

With di-isopropyl azodicarboxylate; water; potassium carbonate; ammonium chloride; benzotriazol-1-ol; dicyclohexyl-carbodiimide; triphenylphosphine; potassium hydroxide; zinc; In tetrahydrofuran; methanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone;
DOI:10.1021/jm3014844