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Technology Process of C43H46Cl2N8O15P2

C43H46Cl2N8O15P2

Base Information
  • Chemical Name:C43H46Cl2N8O15P2
  • CAS No.:91593-05-4
  • Molecular Formula:C43H46Cl2N8O15P2
  • Molecular Weight:1047.74
  • Hs Code.:
C<sub>43</sub>H<sub>46</sub>Cl<sub>2</sub>N<sub>8</sub>O<sub>15</sub>P<sub>2</sub>

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Chemical Property of C43H46Cl2N8O15P2
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Technology Process of C43H46Cl2N8O15P2

There total 7 articles about C43H46Cl2N8O15P2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-chlorophenyl phosphordi(1H-1-[1,2,4]triazolide)
72351-28-1

2-chlorophenyl phosphordi(1H-1-[1,2,4]triazolide)

C<sub>43</sub>H<sub>46</sub>Cl<sub>2</sub>N<sub>8</sub>O<sub>15</sub>P<sub>2</sub>
91593-05-4

C43H46Cl2N8O15P2

Guidance literature:
Multi-step reaction with 3 steps
1: pyridine / CH2Cl2 / 1 h / Ambient temperature
2: 1-methylimidazole / Ambient temperature
3: 1) 2 percent benzenesulfonic acid; 2) 5 percent sodium bicarbonate / 1) CH2Cl2, MeOH, 0 deg C, 20 min
With pyridine; 1-methyl-1H-imidazole; sodium hydrogencarbonate; benzenesulfonic acid; In dichloromethane;

Reference yield:

5'-O-(4-4'-dimethoxytrityl)thymidine
40615-39-2

5'-O-(4-4'-dimethoxytrityl)thymidine

C<sub>43</sub>H<sub>46</sub>Cl<sub>2</sub>N<sub>8</sub>O<sub>15</sub>P<sub>2</sub>
91593-05-4

C43H46Cl2N8O15P2

Guidance literature:
Multi-step reaction with 3 steps
1: pyridine / CH2Cl2 / 1 h / Ambient temperature
2: 1-methylimidazole / Ambient temperature
3: 1) 2 percent benzenesulfonic acid; 2) 5 percent sodium bicarbonate / 1) CH2Cl2, MeOH, 0 deg C, 20 min
With pyridine; 1-methyl-1H-imidazole; sodium hydrogencarbonate; benzenesulfonic acid; In dichloromethane;

Reference yield:

C<sub>64</sub>H<sub>64</sub>Cl<sub>2</sub>N<sub>8</sub>O<sub>17</sub>P<sub>2</sub>

C64H64Cl2N8O17P2

C<sub>43</sub>H<sub>46</sub>Cl<sub>2</sub>N<sub>8</sub>O<sub>15</sub>P<sub>2</sub>
91593-05-4

C43H46Cl2N8O15P2

Guidance literature:
With sodium hydrogencarbonate; benzenesulfonic acid; Multistep reaction; 1) CH2Cl2, MeOH, 0 deg C, 20 min;
upstream raw materials:

5'-O-dimethoxytrityl-N-isobutyryldeoxyguanosine

2-chlorophenyl phosphordi(1H-1-[1,2,4]triazolide)

N-isobutyryl-3'-O-(o-chlorophenyl)(p-methoxyanilido)phospho-deoxyguanosine

[1,2,4]Triazol-1-yl-phosphonic acid (2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester 2-chloro-phenyl ester

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