pref-3-Methoxy-1,4-diphenyl-2-butanol

Base Information

• Chemical Name: pref-3-Methoxy-1,4-diphenyl-2-butanol
• CAS No.: 92695-16-4
• Molecular Formula: C₁₇H₂₀O₂
• Molecular Weight: 256.345
• Mol file: 92695-16-4.mol

Synonyms:

Chemical Property of pref-3-Methoxy-1,4-diphenyl-2-butanol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of pref-3-Methoxy-1,4-diphenyl-2-butanol

There total 5 articles about pref-3-Methoxy-1,4-diphenyl-2-butanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trans,trans-1,4-Diphenyl-1,3-butadiene (886-65-7,538-81-8) → pref-3-Methoxy-1,4-diphenyl-2-butanol (92695-16-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 3.5 g / Na / diethyl ether; H₂O

2: 0.97 g / m-chloroperoxybenzoic acid / CHCl₃ / 1) -20 deg C, 1h 2) 5 deg C, 24h

3: 0.08 g / 0.2N H₂SO₄ / methanol / 24 h / Ambient temperature; Na, CH₃OH, 24h;

With sulfuric acid; sodium; 3-chloro-benzenecarboperoxoic acid; In methanol; diethyl ether; chloroform; water;

DOI:10.1021/jo00198a024

Reference yield:

(E)-1,4-diphenylbut-2-ene (1142-22-9) → pref-3-Methoxy-1,4-diphenyl-2-butanol (92695-16-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 0.97 g / m-chloroperoxybenzoic acid / CHCl₃ / 1) -20 deg C, 1h 2) 5 deg C, 24h

2: 0.08 g / 0.2N H₂SO₄ / methanol / 24 h / Ambient temperature; Na, CH₃OH, 24h;

With sulfuric acid; 3-chloro-benzenecarboperoxoic acid; In methanol; chloroform;

DOI:10.1021/jo00198a024

Reference yield:

phenylacetaldehyde (122-78-1) → pref-3-Methoxy-1,4-diphenyl-2-butanol (92695-16-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 0.8 g / butyllithium

2: 0.97 g / m-chloroperoxybenzoic acid / CHCl₃ / 1) -20 deg C, 1h 2) 5 deg C, 24h

3: 0.08 g / 0.2N H₂SO₄ / methanol / 24 h / Ambient temperature; Na, CH₃OH, 24h;

With n-butyllithium; sulfuric acid; 3-chloro-benzenecarboperoxoic acid; In methanol; chloroform;

DOI:10.1021/jo00198a024

upstream raw materials:

methanol

trans-2,3-Dibenzyloxirane

trans,trans-1,4-Diphenyl-1,3-butadiene

(E)-1,4-diphenylbut-2-ene