2-(7-methoxy-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl)-5-pyrrolidin-1-ylaniline

Base Information

Chemical Name:2-(7-methoxy-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl)-5-pyrrolidin-1-ylaniline
CAS No.:1189352-73-5
Molecular Formula:C₁₈H₂₃N₃OS
Molecular Weight:329.466
Hs Code.:

Synonyms:

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Chemical Property of 2-(7-methoxy-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl)-5-pyrrolidin-1-ylaniline

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Technology Process of 2-(7-methoxy-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl)-5-pyrrolidin-1-ylaniline

There total 4 articles about 2-(7-methoxy-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl)-5-pyrrolidin-1-ylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 1189352-72-4
2-(2-nitro-4-pyrrolidin-1-ylphenyl)-4,5,6,7-tetrahydro-1,3-benzothiazol-7-ol

: 1189352-73-5
2-(7-methoxy-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl)-5-pyrrolidin-1-ylaniline

Guidance literature:: With iron; acetic acid; for 0.5h; Reflux;

Reference yield:

: 80517-21-1
4-fluoro-2-nitrobenzonitrile

: 1189352-73-5
2-(7-methoxy-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl)-5-pyrrolidin-1-ylaniline

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / 2 h / 20 °C

2: methanol; tetraphosphorus decasulfide / 72 h / 20 °C / Inert atmosphere

3: tetraphosphorus decasulfide; ethanol / 2 h / 60 °C

4: iron; acetic acid / 0.5 h / Reflux

With methanol; tetraphosphorus decasulfide; ethanol; iron; acetic acid; In tetrahydrofuran;

Reference yield:

: 1189353-71-6
2-nitro-4-pyrrolidin-1-ylbenzonitrile

: 1189352-73-5
2-(7-methoxy-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl)-5-pyrrolidin-1-ylaniline

Guidance literature:: Multi-step reaction with 3 steps

1: methanol; tetraphosphorus decasulfide / 72 h / 20 °C / Inert atmosphere

2: tetraphosphorus decasulfide; ethanol / 2 h / 60 °C

3: iron; acetic acid / 0.5 h / Reflux

With methanol; tetraphosphorus decasulfide; ethanol; iron; acetic acid;