3-Phenyl-4H-1-benzothiopyran-4-one

Base Information

Chemical Name:3-Phenyl-4H-1-benzothiopyran-4-one
CAS No.:4430-54-0
Molecular Formula:C15H10 O S
Molecular Weight:238.31
Hs Code.:
DSSTox Substance ID:DTXSID301295453

Synonyms:3-Phenyl-4H-1-benzothiopyran-4-one;4430-54-0;SCHEMBL9246481;DTXSID301295453

Suppliers and Price of 3-Phenyl-4H-1-benzothiopyran-4-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-Phenyl-4H-1-benzothiopyran-4-one

Chemical Property:

XLogP3:3.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:238.04523611
Heavy Atom Count:17
Complexity:328

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2=CSC3=CC=CC=C3C2=O

Technology Process of 3-Phenyl-4H-1-benzothiopyran-4-one

There total 9 articles about 3-Phenyl-4H-1-benzothiopyran-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: C₁₅H₁₂O₂S

: 4430-54-0
3-phenyl-4H-thiochromen-4-one

Guidance literature:: In trifluorormethanesulfonic acid; at 120 ℃; for 3h;
DOI:10.1021/acscatal.9b02982

Reference yield: 71.0%

: 201230-82-2
carbon monoxide

: 536-74-3
phenylacetylene

: 882-33-7
diphenyldisulfane

: 4430-54-0
3-phenyl-4H-thiochromen-4-one

Guidance literature:: With chloro(1,5-cyclooctadiene)rhodium(I) dimer; bis(1-methyl-1-phenylethyl)peroxide; triphenylphosphine; lithium bromide; In N,N-dimethyl acetamide; at 110 ℃; for 24h; under 3750.38 Torr; Reagent/catalyst; Solvent; Catalytic behavior; Autoclave; Sealed tube;
DOI:10.1021/acs.joc.8b02294

Reference yield: 68.0%

: 201230-82-2
carbon monoxide

: 108-98-5
thiophenol

: 536-74-3
phenylacetylene

: 4430-54-0
3-phenyl-4H-thiochromen-4-one

Guidance literature:: With chloro(1,5-cyclooctadiene)rhodium(I) dimer; di-tert-butyl peroxide; tetra-(n-butyl)ammonium iodide; triphenylphosphine; In 1-methyl-pyrrolidin-2-one; at 110 ℃; for 24h; under 3750.38 Torr; Sealed tube; Autoclave;
DOI:10.1021/acs.joc.8b02294