Technology Process of C57H84N6O14
There total 24 articles about C57H84N6O14 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
4-methyl-morpholine; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide;
Ambient temperature;
DOI:10.1021/ja00256a046
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 89 percent / EDC / 0 °C
2: 80 percent / H2 / 10percent Pd/C / acetic acid
3: 89 percent / DMAP, DCC / 0 °C
4: 8N HCl / ethyl acetate / Ambient temperature
5: 56 percent / HOBt, EDC / 0 °C
6: 95 percent / Bu4N(1+)*F(1-) / Ambient temperature
7: 99 percent / TFA-OH / 0 °C
8: 8 percent / NMM, HOBt, EDC / Ambient temperature
With
4-methyl-morpholine; hydrogenchloride; dmap; tetrabutyl ammonium fluoride; hydrogen; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; dicyclohexyl-carbodiimide; trifluoroacetic acid;
palladium on activated charcoal;
In
acetic acid; ethyl acetate;
DOI:10.1021/ja00256a046
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 71 percent / HOBt, DCC / 0 °C
2: H2 / 10percent Pd/C / propan-2-ol
3: 84 percent / DMAP, DCC / 0 °C
4: 95 percent / Bu4N(1+)*F(1-) / Ambient temperature
5: 56 percent / HOBt, EDC / 0 °C
6: 95 percent / Bu4N(1+)*F(1-) / Ambient temperature
7: 99 percent / TFA-OH / 0 °C
8: 8 percent / NMM, HOBt, EDC / Ambient temperature
With
4-methyl-morpholine; dmap; tetrabutyl ammonium fluoride; hydrogen; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; dicyclohexyl-carbodiimide; trifluoroacetic acid;
palladium on activated charcoal;
In
isopropyl alcohol;
DOI:10.1021/ja00256a046
