3--crotonsaeure-tert.-butylamid

Base Information

• Chemical Name: 3--crotonsaeure-tert.-butylamid
• CAS No.: 19625-78-6
• Molecular Formula: C₁₈H₂₄N₂O₅
• Molecular Weight: 348.399

Synonyms:

Chemical Property of 3--crotonsaeure-tert.-butylamid

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 3--crotonsaeure-tert.-butylamid

There total 2 articles about 3--crotonsaeure-tert.-butylamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-t-Butylimino-3-buten-2-one (10513-47-0) + N-(Benzyloxycarbonyl)glycine (1138-80-3) → 3--crotonsaeure-tert.-butylamid (19625-78-6)

Guidance literature:

In tetrachloromethane;

DOI:10.1021/ja01007a060

Reference yield:

2-tert-butyl-5-methylisoxazolium perchlorate (10513-45-8) + N-(Benzyloxycarbonyl)glycine (1138-80-3) → 3--crotonsaeure-tert.-butylamid (19625-78-6)

Guidance literature:

With triethylamine; In acetonitrile;

DOI:10.1021/jo00826a020

Reference yield:

3--crotonsaeure-tert.-butylamid (19625-78-6) + tert-butylamine (75-64-9) → benzyl N-[(tert-butylcarbamoyl)methyl]carbamate (21995-76-6)

Guidance literature:

In acetonitrile;

DOI:10.1021/jo00826a020

upstream raw materials:

4-t-Butylimino-3-buten-2-one

N-(Benzyloxycarbonyl)glycine

2-tert-butyl-5-methylisoxazolium perchlorate

Downstream raw materials:

benzyl N-[(tert-butylcarbamoyl)methyl]carbamate

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