N-1-cyclohexenyl-N-methylcarbamyl chloride

Base Information

• Chemical Name: N-1-cyclohexenyl-N-methylcarbamyl chloride
• CAS No.: 33542-26-6
• Molecular Formula: C₈H₁₂ClNO
• Molecular Weight: 173.642
• Mol file: 33542-26-6.mol

Synonyms:

Chemical Property of N-1-cyclohexenyl-N-methylcarbamyl chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-1-cyclohexenyl-N-methylcarbamyl chloride

There total 3 articles about N-1-cyclohexenyl-N-methylcarbamyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bis(trichloromethyl) carbonate (32315-10-9) + N-cyclohexylidenemethylamine (6407-35-8) → N-1-cyclohexenyl-N-methylcarbamyl chloride (33542-26-6)

Guidance literature:

bis(trichloromethyl) carbonate; With pyridine; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere;

N-cyclohexylidenemethylamine; In dichloromethane; at 0 ℃; for 2h; Inert atmosphere;

DOI:10.1021/ja301591m

Reference yield:

phosgene (75-44-5) + N-cyclohexylidenemethylamine (6407-35-8) → N-1-cyclohexenyl-N-methylcarbamyl chloride (33542-26-6)

Guidance literature:

In benzene;

Reference yield:

→ N-1-cyclohexenyl-N-methylcarbamyl chloride (33542-26-6)

Guidance literature:

Imin /BRN= 446196/, Phosgen;

upstream raw materials:

phosgene

N-cyclohexylidenemethylamine

bis(trichloromethyl) carbonate

Downstream raw materials:

1-cyclohexen-1-yl-1,3-dimethyl-3-[(1S)-1-phenylethyl]urea