(4-fluoro-2-iodo-phenoxy)-acetic acid

Base Information

Chemical Name:(4-fluoro-2-iodo-phenoxy)-acetic acid
CAS No.:451-91-2
Molecular Formula:C₈H₆FIO₃
Molecular Weight:296.037
Hs Code.:

Synonyms:

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Chemical Property of (4-fluoro-2-iodo-phenoxy)-acetic acid

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Technology Process of (4-fluoro-2-iodo-phenoxy)-acetic acid

There total 5 articles about (4-fluoro-2-iodo-phenoxy)-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 459-60-9
1-fluoro-4-methoxybenzene

: 451-91-2
(4-fluoro-2-iodo-phenoxy)-acetic acid

Guidance literature:: Multi-step reaction with 5 steps

1: fuming nitric acid; acetic acid; acetic acid anhydride

2: iron

3: aqueous sulfuric acid; sodium nitrite / Erwaermen der Reaktionsloesung mit Kaliumjodid

4: aqueous hydriodic acid; acetic acid anhydride

5: aq. NaOH solution

With sodium hydroxide; sulfuric acid; hydrogen iodide; nitric acid; acetic anhydride; iron; acetic acid; sodium nitrite;
DOI:10.1021/ja01510a021

Reference yield:

: 1978-39-8
5-fluoro-2-methoxy-aniline

: 451-91-2
(4-fluoro-2-iodo-phenoxy)-acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: aqueous sulfuric acid; sodium nitrite / Erwaermen der Reaktionsloesung mit Kaliumjodid

2: aqueous hydriodic acid; acetic acid anhydride

3: aq. NaOH solution

With sodium hydroxide; sulfuric acid; hydrogen iodide; acetic anhydride; sodium nitrite;
DOI:10.1021/ja01510a021

Reference yield:

: 3824-22-4
4-fluoro-2-iodo-1-methoxybenzene

: 451-91-2
(4-fluoro-2-iodo-phenoxy)-acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: aqueous hydriodic acid; acetic acid anhydride

2: aq. NaOH solution

With sodium hydroxide; hydrogen iodide; acetic anhydride;
DOI:10.1021/ja01510a021