C₂₅H₂₄O₈

Base Information

• Chemical Name: C₂₅H₂₄O₈
• CAS No.: 76649-98-4
• Molecular Formula: C₂₅H₂₄O₈
• Molecular Weight: 452.461
• Mol file: 76649-98-4.mol

Synonyms:

Chemical Property of C₂₅H₂₄O₈

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₅H₂₄O₈

There total 1 articles about C₂₅H₂₄O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(+)-Daunomycinone (21794-55-8) + 2,2-dimethoxy-propane (77-76-9) → C25H24O8 (76649-98-4) + C22H20O8

Guidance literature:

With toluene-4-sulfonic acid; In chloroform; Heating;

DOI:10.1016/0040-4020(95)00892-C

Reference yield:

C25H24O8 (76649-98-4) → C41H42O10 (76650-02-7)

Guidance literature:

Multi-step reaction with 4 steps

1: 100 percent / m-chloroperbenzoic acid / CHCl₃ / Ambient temperature

2: 70 percent Chromat_. / KI / dimethylformamide; acetone / 3 h / 60 °C

3: p-toluenesulfonic acid

4: NaH / tetrahydrofuran / 6 h / 55 °C

With sodium hydride; 3-chloro-benzenecarboperoxoic acid; potassium iodide; toluene-4-sulfonic acid; In tetrahydrofuran; chloroform; N,N-dimethyl-formamide; acetone;

DOI:10.1016/0040-4039(80)80017-7

Reference yield:

C25H24O8 (76649-98-4) → C40H40O10 (76649-99-5,76704-60-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 100 percent / m-chloroperbenzoic acid / CHCl₃ / Ambient temperature

2: 70 percent Chromat_. / KI / dimethylformamide; acetone / 3 h / 60 °C

3: p-toluenesulfonic acid

With 3-chloro-benzenecarboperoxoic acid; potassium iodide; toluene-4-sulfonic acid; In chloroform; N,N-dimethyl-formamide; acetone;

DOI:10.1016/0040-4039(80)80017-7

upstream raw materials:

(+)-Daunomycinone

2,2-dimethoxy-propane

Downstream raw materials:

C₃₉H₃₆O₉

C₄₁H₄₂O₁₀

C₄₀H₄₀O₁₀

C₄₀H₄₀O₁₀