[Mn₂(2-hydroxybenzoate)4(OH)4]

Base Information

• Chemical Name: [Mn₂(2-hydroxybenzoate)4(OH)4]
• CAS No.: 905594-45-8
• Molecular Formula: C₂₈H₂₄Mn₂O₁₆
• Molecular Weight: 726.365
• Mol file: 905594-45-8.mol

Synonyms:

Chemical Property of [Mn₂(2-hydroxybenzoate)4(OH)4]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [Mn₂(2-hydroxybenzoate)4(OH)4]

There total 1 articles about [Mn₂(2-hydroxybenzoate)4(OH)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

manganese (II) acetate tetrahydrate (6156-78-1) + salicylaldehyde (90-02-8) + salicylic acid (69-72-7,25496-36-0,8052-31-1) → [Mn2(2-hydroxybenzoate)4(OH)4] (905594-45-8)

Guidance literature:

With glycine; NaOH; pyridine; In methanol; ethanol; water; glycine in hot H2O added to HOC6H4CHO in hot EtOH, refluxed (1 h), cooled, filtered, ppt. washed (EtOH), dissolved in 90% EtOH; HOC6H4COOH in MeOH added to NaOH in MeOH; solns. added successively to Mn salt in MeOH with stirring (40°C, 45 min); pyridine added dropwise with stirring; stirred at 45°C for 45 min; concd.; crystd. at room temp. for 10 d; elem. anal.;

DOI:10.1016/j.ica.2004.11.044

upstream raw materials:

manganese (II) acetate tetrahydrate

salicylaldehyde

salicylic acid